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← Document results/DEP Box 27/GCMS X 4/10/02 A 4/15/02
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GCMS analysis results, Sample AE05750, April 18, 2002

Machine-extracted title · confidence 100%

Reference standard analysis results for volatile organic compounds used to verify GCMS instrument performance.

NYC-WTC_000048500–000048511

Folder label: “GCMS X 4/10/02 A 4/15/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR1202\5750.D Vial: 19 Acq On : 16 Apr 2002 1:43 am Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 17 9:37 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Apr 16 14:55:12 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.60 178 408 N.D. 35) Anthracene 25.60 178 408 N.D. 36) Di-n-butylphthalate 27.59 149 3510 N.D. 37) Fluoranthene 0.00 202 0 N.D. 40) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 32.09 149 520 N.D. 42) Benzo(a)anthracene 33.66 228 2652 N.D. 43) Bis(2-ethylhexyl)phthalate 33.88 149 7376 0.34 ug/1 # 98 44) Chrysene 33.73 228 1029 N.D. 46) Di-n-Octylphthalate 35.62 149 484 N.D. 47) Benzo(b)fluoranthene 36.72 252 656 N.D. 48) Benzo(k)fluoranthene 36.79 252 820 N.D. 49) Benzo(a)pyrene 37.90 252 2395 N.D. 50) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 5750.D GCMS0412.M Wed Apr 17 09:38:43 2002 Page 2

NYC-WTC_000048503

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NYC-WTC_000048503Source: NYC Law Department, mirrored locally

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