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GCMS analysis results, Sample AE08270, April 22, 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08270 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048456–000048465

Folder label: “GCMS X 4/9/02 A 4/17/02

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Scanned page image, NYC-WTC_000048461
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\APR18 02\8 2 7 0.D Vial: 4 Acq On 18 Apr 2002 2:54 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK• peak peak peak % of # min scan scan scan TY height area % max. total

1 8.191 339 343 369 rVB 272293 678280 21.83% 4.112% 2 12.212 776 781 798 rVB 952093 2310480 74.36% 14.008% 3 14.810 1059 1064 1070 rBB 142266 265270 8.54% 1.608% 4 15.848 1171 1177 1192 rBV 1388586 2848073 91.66% 17.268% 5 21.145 1748 1754 1771 rBV 1521277 3107226 100.00% 18.839%

6 23.284 1981 1987 1993 rVB 167036 323852 10.42% 1.963% 7 25.588 2232 2238 2250 rBV2 1438555 2948198 94.88% 17.875% 8 33.639 3109 3115 3135 rBV2 1008015 2269158 73.03% 13.758% 9 37.871 3568 3576 3595 rBV2 604790 1743138 56.10% 10.569%

Sum of corrected areas: 16493675 8270 .D GCMS0412.M Fri Apr 19 08:30:54 2002

NYC-WTC_000048461

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NYC-WTC_000048461Source: NYC Law Department, mirrored locally

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