GCMS analysis results, Sample AE08266, April 22, 2002

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GCMS analysis report for sample AE08266 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048401–000048420

Folder label: “GCMS X 4/9/02 A 4/17/02”

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NYC 9/11 Public Portal Document

'88 21.623 3153 3156 3159 W 3 3162 43768 0.06% 0.012% 89 21.822 3180 3190 3194 W 3 18792 364192 0.53% 0.098% 90 21.864 3194 3197 3204 W 5 7247 147717 0.21% 0.040%

91 22.087 3232 3235 3241 W 2123 27333 0.04% 0.007% 92 22.234 3253 3260 3266 W 2 2014 45844 0.07% 0.012% 93 22.369 3281 3283 3285 W 2514 16885 0.02% 0.005% 94 22.563 3311 3316 3319 W 2 3638 60621 0.09% 0.016% 95 22.639 3319 3329 3338 W 2 30711 610825 0.88% 0.165%

96 22.704 3338 3340 3351 W 4 2452 70381 0.10% 0.019% 97 22.786 3351 3354 3359 W 2295 37184 0.05% 0.010% 98 23.021 3383 3394 3414 W 2 3177038 69074603 100.00% 18.651% 99 23.174 3414 3420 3429 W 40759 1003016 1.45% 0.271% 100 23.238 3429 3431 3433 W 3 5643 70540 0.10% 0.019%

101 23.256 3433 3434 3436 W 2 5486 53975 0.08% 0.015% 102 23.468 3467 3470 3471 W 3077 28804 0.04% 0.008% 103 23.720 3507 3513 3520 W 4 2633 72017 0.10% 0.019% 104 24.173 3581 3590 3598 W 2 3582 109452 0.16% 0.030% 105 24.255 3601 3604 3614 W 2435 59327 0.09% 0.016%

106 25.154 3747 3757 3764 W 3 12460 265005 0.38% 0.072% 107 26.981 4063 4068 4071 W 2082 29288 0.04% 0.008% 108 27.028 4074 4076 4081 W 2 1965 24705 0.04% 0.007% 109 28.597 4335 4343 4345 W 2 1875 39453 0.06% 0.011% 110 29.543 4497 4504 4507 W 2072 37830 0.05% 0.010%

ill 29.772 4539 4543 4545 W 2034 26809 0.04% 0.007% 112 30.048 4575 4590 4602 W 5 4295 180225 0.26% 0.049% 113 30.595 4680 4683 4685 PV 2 1705 21216 0.03% 0.006% 114 30.888 4717 4733 4761 W 2 2444794 56408718 81.66% 15.231% 115 31.065 4761 4763 4767 W 3 6232 101903 0.15% 0.028%

116 31.100 4767 4769 4772 W 3 4727 66897 0.10% 0.018% 117 31.141 4772 4776 4787 W 5 6476 239482 0.35% 0.065% 118 31.458 4823 4830 4843 PV 3 12532 353395 0.51% 0.095% 119 31.547 4843 4845 4854 W 4 1839 25051 0.04% 0.007% 120 32.710 5041 5043 5045 W 2212 16815 0.02% 0.005%

121 33.086 5103 5107 5110 PV 1703 24165 0.03% 0.007% 122 33.133 5110 5115 5118 W 2 2018 33412 0.05% 0.009% 123 33.468 5167 5172 5174 W 2 1917 30053 0.04% 0.008% 124 33.532 5180 5183 5190 PV 1537 24386 0.04% 0.007% 125 34.790 5379 5397 5444 PV 2 1674527 43452420 62.91% 11.733%

126 35.084 5444 5447 5450 W 3 4886 93401 0.14% 0.025% 127 35.113 5450 5452 5456 W 2 4320 80484 0.12% 0.022% 128 35.154 5456 5459 5464 W 5 3627 87766 0.13% 0.024% 129 35.207 5464 5468 5478 W 4 3757 139196 0.20% 0.038% 130 35.589 5532 5533 5538 W 4 3037 40583 0.06% 0.011%

131 35.689 5547 5550 5552 W 2792 32390 0.05% 0.009% 132 35.718 5552 5555 5559 W 3 3127 56978 0.08% 0.015% 133 35.765 5559 5563 5567 W 2 3055 70308 0.10% 0.019% 134 36.053 5609 5612 5614 W 2 3015 38303 0.06% 0.010% 135 36.100 5619 5620 5626 W 3463 63740 0.09% 0.017%

136 36.182 5632 5634 5644 W 3 2708 87667 0.13% 0.024% 137 36.647 5707 5713 5715 W 2 3593 77028 0.11% 0.021%

08266.D 041702SCAN.M Thu Apr 18 09:59:55 2002 Page 3

NYC-WTC_000048407

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NYC-WTC_000048407Source: NYC Law Department, mirrored locally

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GCMS analysis results, Sample AE08264, April 22, 2002 · Box DEP Box 27

NYC-WTC_000048355

GCMS analysis report for sample AE08264 showing surrogate recovery and unknown compound screening on April 22, 2002.

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