GCMS Analysis Results, Sample AE08261, April 22, 2002

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88 25.195 3763 3764 3771 W 2708 37959 0.05% 0.009% 89 25.377 3786 3795 3802 PV 1940 48807 0.06% 0.012% 90 25.824 3868 3871 3881 PV 1752 40161 0.05% 0.010%

91 26.065 3908 3912 3916 W 2 2372 25890 0.03% 0.006% 92 27.551 4161 4165 4169 W 5 4048 75868 0.10% 0.018% 93 28.491 4319 4325 4327 PV 1902 24423 0.03% 0.006% 94 28.626 4338 4348 4350 W 2066 40614 0.05% 0.010% 95 29.778 4540 4544 4547 W 1515 24114 0.03% 0.006%

96 30.060 4576 4592 4600 PV 6 3939 129460 0.17% 0.031% 97 30.495 4663 4666 4671 W 1856 16510 0.02% 0.004% 98 30.888 4721 4733 4765 W 2 2758639 64391160 85.15% 15.522% 99 31.082 4765 4766 4773 W 4 7374 165804 0.22% 0.040% 100 31.141 4773 4776 4790 W 7 4728 220323 0.29% 0.053%

101 31.458 4820 4830 4843 W 5 10842 400764 0.53% 0.097% 102 32.481 5001 5004 5011 PV 3 2073 49239 0.07% 0.012% 103 32.616 5025 5027 5033 W 2 2013 28448 0.04% 0.007% 104 32.663 5033 5035 5040 W 2009 30635 0.04% 0.007% 105 33.051 5098 5101 5104 W 2280 23218 0.03% 0.006%

106 33.139 5114 5116 5119 W 2 1560 15802 0.02% 0.004% 107 33.198 5119 5126 5131 W 2 1666 33618 0.04% 0.008% 108 33.274 5136 5139 5144 PV 2 1914 21258 0.03% 0.005% 109 33.738 5213 5218 5221 PV 1656 23064 0.03% 0.006% 110 33.926 5240 5250 5268 W 104466 3665446 4.85% 0.884%

ill 34.038 5268 5269 5279 W 4 17363 511667 0.68% 0.123% 112 34.102 5279 5280 5285 W 5 9555 201063 0.27% 0.048% 113 34.143 5285 5287 5294 W 2 8172 207230 0.27% 0.050% 114 34.619 5365 5368 5370 W 2 2722 37456 0.05% 0.009% 115 34.796 5382 5398 5434 W 2 2034449 52068722 68.85% 12.552%

116 35.019 5434 5436 5438 W 8679 106738 0.14% 0.026% 117 35.037 5438 5439 5441 W 2 6920 75128 0.10% 0.018% 118 35.054 5441 5442 5467 W 4 6666 391682 0.52% 0.094% 119 35.424 5503 5505 5513 W 3 2917 76366 0.10% 0.018% 120 35.483 5513 5515 5526 W 3 3607 107830 0.14% 0.026%

121 35.589 5526 5533 5536 W 3 3089 86537 0.11% 0.021% 122 35.830 5561 5574 5576 W 3 3479 134138 0.18% 0.032% 123 36.000 5594 5603 5605 W 3159 91213 0.12% 0.022% 124 36.030 5605 5608 5610 W 2 3165 46980 0.06% 0.011% 125 36.118 5621 5623 5626 W 3984 49298 0.07% 0.012%

126 36.300 5652 5654 5658 W 3835 55162 0.07% 0.013% 127 36.458 5678 5681 5686 W 3435 76070 0.10% 0.018% 128 36.664 5713 5716 5717 W 3480 37563 0.05% 0.009% 129 36.846 5744 5747 5750 W 3399 61294 0.08% 0.015% 130 36.923 5758 5760 5765 W 3711 64462 0.09% 0.016%

131 37.716 5892 5895 5897 W 3613 37495 0.05% 0.009% 132 38.309 5992 5996 6002 W 3 2573 61176 0.08% 0.015% 133 38.574 6035 6041 6045 W 2 2556 67300 0.09% 0.016% 134 38.609 6045 6047 6048 W 2 2809 26591 0.04% 0.006% 135 38.738 6067 6069 6075 W 2523 40209 0.05% 0.010%

136 38.891 6090 6095 6098 W 2 3134 48493 0.06% 0.012% 137 39.026 6115 6118 6122 W 2 2413 41873 0.06% 0.010%

08261.D 041702SCAN.M Thu Apr 18 09:47:19 2002 Page 3

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