GCMS surrogate recovery results, April 22 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\020417\08260.D Vial: 17 Acq On : 17 Apr 2002 10:40 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.120 3 7 10 BV 2 12297 160075 0.25% 0.046% 2 3.156 10 13 20 W 4 7917 152117 0.24% 0.044% 3 3.367 42 49 54 PV 15429 231535 0.36% 0.067% 4 3.420 54 58 69 W 10 3584 107655 0.17% 0.031% 5 3.502 69 72 80 W 5 2882 47043 0.07% 0.014%

6 3.573 80 84 87 PV 6 3599 52235 0.08% 0.015% 7 3.602 87 89 91 W 3 2519 25619 0.04% 0.007% 8 3.649 91 97 103 W 22750 382214 0.59% 0.110% 9 3.696 103 105 108 W 3 3508 46378 0.07% 0.013% 10 3.755 108 115 116 W 6 5777 129076 0.20% 0.037%

11 3.778 116 119 128 W 2 10625 244262 0.38% 0.070% 12 4.184 183 188 192 W 5 3709 85608 0.13% 0.025% 13 4.301 203 208 215 W 6 4719 109499 0.17% 0.031% 14 4.372 215 220 221 W 2 2678 37184 0.06% 0.011% 15 4.384 221 222 226 W 2 2843 26255 0.04% 0.008%

16 4.619 258 262 265 W 3 2245 35524 0.06% 0.010% 17 4.783 284 290 296 PV 5 3457 69071 0.11% 0.020% 18 4.883 303 307 314 BV 4 4638 86933 0.13% 0.025% 19 4.983 321 324 327 PV 2 2146 30601 0.05% 0.009% 20 5.053 333 336 346 W 8 2996 64499 0.10% 0.019%

21 5.136 346 350 362 W 5 17646 351719 0.55% 0.101% 22 5.382 390 392 401 W 5 2316 63531 0.10% 0.018% 23 5.465 401 406 411 W 5 2264 34724 0.05% 0.010% 24 5.512 411 414 418 W 5 2259 39296 0.06% 0.011% 25 5.694 440 445 452 W 5 2673 55040 0.09% 0.016%

26 5.964 486 491 497 W 24473 446072 0.69% 0.128% 27 6.029 497 502 516 W 38429 808181 1.25% 0.232% 28 7.280 711 715 717 W 3 1935 22332 0.03% 0.006% 29 7.492 745 751 756 W 2 6953 130227 0.20% 0.037% 30 8.009 835 839 845 PV 2 2164 35320 0.05% 0.010%

31 8.156 859 864 868 W 5 2401 40823 0.06% 0.012% 32 8.861 980 984 992 W 3 5006 88189 0.14% 0.025% 33 9.331 1060 1064 1068 PV 2 2007 22203 0.03% 0.006% 34 9.636 1111 1116 1122 PV 6 3884 80906 0.13% 0.023% 35 9.713 1125 1129 1136 W 3 5117 95992 0.15% 0.028%

36 9.783 1136 1141 1148 W 7 3112 76432 0.12% 0.022% 37 9.983 1164 1175 1195 W 2386391 43926855 68.17% 12.625%

08260.D 041702SCAN.M Thu Apr 18 09:45:49 2002 Page 1

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