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GCMS results sample AE08254, April 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08254 showing surrogate recovery and unknown compounds from April 2002.

NYC-WTC_000047851–000047866

Folder label: “GCMS X 4/8/02 A 4/17/02

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Scanned page image, NYC-WTC_000047853
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020417\08254.D Vial: 12 Acq On : 17 Apr 2002 6:32 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 18 09:15:45 2002 Quant Results File: 041702SCAN.RE

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed Apr 17 08:01:11 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.99 152 7675275 40.00 ug/L -0.02 10) Napthalene-d8 13.49 136 29296272 40.00 ug/L -0.03 17) Acenapthalene-dlO 18.63 164 15913409 40.00 ug/L -0.02 29) Phenanthranene-dlO 23.02 188 24456835 40.00 ug/L -0.02 37) Chrysene-dl2 30.89 240 18792218 40.00 ug/L -0.05 43) Perylene-dl2 34.79 264 13586340 40.00 ug/L -0.02

System Monitoring Compounds 2 7) TCMX 20.60 207 733516 8.31 ug/L 0.00 Spiked Amount 8.000 Recovery = 103.88%

Target Compounds Qvalue 2) n-nitros-dimethyl amine 4.38 74 -1628 Below Cal # 42 35) Di-n-butylphthalate 25.16 149 138047 0.18 ug/L # 96

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08254.D 041702SCAN.M Thu Apr 18 14:07:16 2002 Page 1

NYC-WTC_000047853

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NYC-WTC_000047853Source: NYC Law Department, mirrored locally

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