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GCMS analysis results for sample AE07976, April 18, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07976 conducted on April 18, 2002.

NYC-WTC_000047593–000047607

Folder label: “GCMS X 4/4/02 A 4/15/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020415\07976.D Vial: 16 Acq On : 15 Apr 2002 11:05 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 16 13:45:26 2002 Quant Results File: 041202SCAN.RE

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Tue Apr 16 11:14:47 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.99 152 5492925 40.00 ug/L 0.00 10) Napthalene-d8 13.49 136 20807721 40.00 ug/L -0.01 17) Acenapthalene-dlO 18.63 164 12293102 40.00 ug/L -0.01 29) Phenanthranene-dlO 23.02 188 18918940 40.00 ug/L -0.01 37) Chrysene-dl2 30.88 240 14573792 40.00 ug/L -0.02 43) Perylene-dl2 34.79 264 9782331 40.00 ug/L -0.01

System Monitoring Compounds 2 7) TCMX 20.60 207 440362 6.46 ug/L 0.00 Spiked Amount 8.000 Recovery = 80.75%

Target Compounds Qvalue 35) Di-n-butylphthalate 25.16 149 515110 0.93 ug/L 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 07976.D 041202SCAN.M Tue Apr 16 13:45:54 2002 Page 1

NYC-WTC_000047595

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NYC-WTC_000047595Source: NYC Law Department, mirrored locally

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