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GCMS analysis results for sample AE08252, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08252 conducted on April 19, 2002, including surrogate recovery data.

NYC-WTC_000047802–000047829

Folder label: “GCMS X 4/8/02 A 4/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\020417\08252.D Vial: 10 Acq On 17 Apr 2002 4:52 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 18 09:12:27 2002 Quant Results File: 041702SCAN.RE

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed Apr 17 08:01:11 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.99 152 7097558 40.00 ug/L -0.02 10) Napthalene-d8 13.49 136 27309861 40.00 ug/L -0.03 17) Acenapthalene-dlO 18.63 164 14689197 40.00 ug/L -0.02 29) Phenanthranene-dlO 23.02 188 21874850 40.00 ug/L -0.02 37) Chrysene-dl2 30.88 240 15254048 40.00 ug/L -0.05 43) Perylene-dl2 34.78 264 10327164 40.00 ug/L -0.02

System Monitoring Compounds 27) TCMX 20.60 207 633472 7.78 ug/L 0.00 Spiked Amount 8.000 Recovery 97.25%

Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08252.D 041702SCAN.M Thu Apr 18 14:07:02 2002 Page 1

NYC-WTC_000047804

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NYC-WTC_000047804Source: NYC Law Department, mirrored locally

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