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GCMS calibration table for method GCMS0412, April 2002

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Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.

NYC-WTC_000047701–000047714

Folder label: “GCMS X 4/4/02 A 4/12/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR1102\8016.D Vial: 22 Acq On : 12 Apr 2002 11:02 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Miso Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 16 12:00 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Apr 16 11:47:07 2002 Response via : Initial Calibration DataAcq Meth : GCMS0408

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.62 178 344 N.D. 35) Anthracene 25.62 178 344 N.D. 36) Di-n-butylphthalate 27.57 149 69801 1.63 ug/1 98 37) Fluoranthene 0.00 202 0 N.D. 40) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 32.10 149 479 N.D. 42) Benzo(a)anthracene 33.66 228 1836 N.D. 43) Bis(2-ethylhexyl)phthalate 33.88 149 7442 0.38 ug/1 94 44) Chrysene 33.66 228 1836 N.D. 46) Di-n-Octylphthalate 35.63 149 424 N.D. 47) Benzo(b)fluoranthene 36.72 252 431 N.D. 48) Benzo(k)fluoranthene 36.79 252 326 N.D. 49) Benzo(a)pyrene 37.71 252 545 N.D. 50) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 43.24 276 493 N.D.

(#) = qualifier out of range (m) = manual integration 8016.D GCMS0412.M Tue Apr 16 12:01:07 2002 Page 2

NYC-WTC_000047702

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NYC-WTC_000047702Source: NYC Law Department, mirrored locally

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