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GCMS calibration table for method GCMS0412, April 2002

Machine-extracted title · confidence 100%

Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.

NYC-WTC_000047701–000047714

Folder label: “GCMS X 4/4/02 A 4/12/02

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NYC 9/11 Public Portal Document

thester ENVIRONMENTAL SERVICES SAMPLE SUBMISSION FORM 4o\"ASCO%, rgovcom WESTCHESTER COUNTY LABORATORIES AND RESEARCH 22 S 2 Dana Road, Valhalla, New York 10595 (914)231-1620 Fax (914) 231-1772 fF Ssf0n0* .A seani) — NYS-ELAP No. 10108 Time/Date Set: Form A-70 (rev. 10/01) P ZZ. J,PEC/BEHH7 Sample Type (circle one): J. Potable. 3. Non Potable Treated Bottle #’s: G32 5 219G6S706, Ub 2. Non Potable 4. Other Chain of Custody? _ Yes_ No A k55 i c5%, lo 53 Time/Date Collected: 4/ 1 3 02 " 45 Comments: K e< Rek Collected By: D , ScU Agency Code: PWS #:________ Source ID: Type Descriptor: Collected From: ___ Bill to: Location’s/Individual’s Name. N Y CDEP Name/Company Street C (0s LAKE pRI E____ Street City/St/Zip VALHALLA PY /0590 City/St/Zip Identification of Source______________________________ Phone#: Fax#: Collection Point CA J_ (H CA,CH, Bl? Check#: Amounts.

BACTERIOLOGICAL ANALYSIS Lab#: /) Q/ Lab#:_______________________ ( / A ( ; / 4 ORGANIC POTABLE ANALYSIS ORGANIC NONPOTABLE/SOLID ANALYSIS __ Heterotrophic Plate Count (hemodialysis & all others) __ Trihalomethanes (524) __ Purgeable Halocarbons (624/8260) __ Coliform P/A (Public supplies) Volatile Halocarbons (524) __ Purgeable Aromatics (624/8260) Volatile Aromatics (524) __ Acrolein & Acrylonitrile (8260) __ Coliform MPN (priv well, raw, stp) __ Fecal Coliform (all samples) Total Trihalomethane Potential (510) __ Organochlorine Pesticides (608/8081) __ Microscopic Microextractables (504) PCB’s (Arochlors) (608/8081) __ Macroscopic __ Pesticides/PCB screen (508) _ Herbicides (SM18/6630,8151) _ API PCB as Decachlorobiphenyl (508A) __ Other Pesticides (SM18/6630) __ Other:_____________________ __ Herbicides (515) __ Petroleum Hydrocarbon Scan (310-13) Pesticides (525) __ Glycols in Water Refrigerated?yes no __ Carbamate Pesticides (531) __ Acid Extractables (625/8270) 1 Chlorinated:? yes no __ Glyphosate (547) Base Neutral Extractables (625/8270) Diquat (549) XGC/MS Unknown Scan Free Chlorine Res: . mg/L Chlorination Disinfection Byproducts (551) Phthalates (606MS) Total Chlorine Res: mg/L __ Haloacetic Acids (552) __ Other:____________________________ _ Other Pesticides (SM18/6630) pH ___________ _UCMRList1 RADIOCHEMICAL ANALYSIS _ MtBE Only (524) Radon __ Other____________________

INORGANIC ANALYSIS REQUESTED - Lab#: __ Color __ Acidity ./Aluminum __ Potassium __ Turbidity *_ Alkalinity 7Antimony A Selenium _ PH __ Bromide X Arsenic Silver ■ ( J ; __ Conductivity __ Bromate/Chlorate/Chlorite Barium __ Sodium; //; 1 45 Corrosivity (temp: °C) Chloride X Beryllium X Thallium l __ BOD (5 day) __ Cyanide Boron __ Vanadium ■ __ Carbonaceous BOD (5 day) __ Fluoride Cadmium AZinc ; __ Soluble BOD (5 day) __ Hardness, Total as CaC03 'Calcium, as CaCOs __ Chemical Oxygen Demand CLP ; __ Nitrogen, Ammonia as N __ Calcium, Ca+2 __ Dissolved Oxygen __ Nitrogen, Nitrate as N __ Metals/CN X Chromium, Total __ Total Organic Carbon __ Volatiles __ Nitrogen, Nitrite as N _ Chromium, Hexavalent __ Total Organic Halides __ Semi-violatiles __ Nitrogen, Total Kjeldahl as N X Cobalt __ Solids, Percent (%) __ Pesticides/PCB’s __ Oil and Grease K Cooper __ Solids, Settleable __ Phenol > Iron __ Solids, Suspended TCLP __ Phosphorus Total as P < Lead __ Solids, Total __ TCLP-Metals __ Phosphorus, Ortho as P __ Magnesium __ Solids, Total Dissolved __ TCLP-Pesticides __ Sulfates X Manganese __ Solids, Total Volatile _TCLP-Herbicides __ Surfactants / Mercury A Other:6 n X Molybdenum __ TCLP-Volatiles _ UV254 __ TCLP-BNA’s 7 Nickel

NYC-WTC_000047714

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NYC-WTC_000047714Source: NYC Law Department, mirrored locally

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