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GCMS analysis results for sample AE07977, April 18, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07977 conducted on April 18, 2002.

NYC-WTC_000047608–000047623

Folder label: “GCMS X 4/4/02 A 4/15/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020415\07977.D Vial: 17 Acq On 15 Apr 2002 11:54 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 16 13:46:35 2002 Quant Results File: 041202SCAN.RE

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Tue Apr 16 11:14:47 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.99 152 6274016 40.00 ug/L 0.00 10) Napthalene-d8 13.49 136 23603950 40.00 ug/L -0.01 17) Acenapthalene-dlO 18.63 164 13901518 40.00 ug/L 0.00 29) Phenanthranene-dlO 23.02 188 21416264 40.00 ug/L 0.00 37) Chrysene-dl2 30.89 240 16204674 40.00 ug/L -0.02 43) Perylene-dl2 34.79 264 10782045 40.00 ug/L -0.01

System Monitoring Compounds 2 7) TCMX 20.60 207 482699 6.26 ug/L 0.00 Spiked Amount 8.000 Recovery 78.25%

Target Compounds Qvalue 35) Di-n-butylphthalate 25.16 149 530367 0.85 ug/L 98

(#) = qualifier out of range (m) = manual integration (+) = signals summed 07977.D 041202SCAN.M Tue Apr 16 13:46:54 2002 Page 1

NYC-WTC_000047610

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NYC-WTC_000047610Source: NYC Law Department, mirrored locally

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