GCMS method parameters and quality control data, April 2002

NYC 9/11 Public Portal Document

DFTPP

Data File C:\MSDCHEM\l\DATA\020404\DFTPPl.D Vial: 1 Acq On 4 Apr 2002 8:00 am Operator: Nefliu Sample df tpp Inst Instrume Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Method : C:\MSDCHEM\1\METHODS\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan

Abundance TIC: DFTPP1.D

3000000

2000000

1000000

0— I । 1 1 1 1 1 1 1 1 1 Time-> 16.00 16.50 17.00 17.50 18.00 18.50 19.00 19.50 Abundance Average of 17.790 to 17.813 min.: DFTPP1.D 250000 198 442 200000

150000 127 255 77 100000 51 110 275 50000 224 j 93 148 167,.L | 1.226 323 346 365 383 403 423 , , m/z-> 0 -34 +t +814444241 I ^1 ( I fl | I I I-1-| 1 I l 'I | ‘l 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440 Frmi | A > I ■ | TH l 11 I . I M I I I j1

Spectrum Information: Average of 17.790 to 17.813 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 35.5 87752 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 37.8 93240 PASS 70 69 0.00 2 0.5 451 PASS 127 198 40 60 51.7 127568 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 246941 PASS 199 198 5 9 6.7 16510 PASS 275 198 10 30 24.5 60506 PASS 365 198 1 99 3.1 7546 PASS 441 443 1 100 87.6 37741 PASS 442 198 40 110 89.3 220432 PASS 443 442 17 23 19.6 43101 PASS

DFTPP1.D SCANAPR0902.M Wed Apr 10 15:04:11 2002

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