GCMS method documentation fragment, April 2002

NYC 9/11 Public Portal Document

DFTPP

Data File C:\MSDCHEM\l\DATA\020415\DFTPPl.D vial: 1 Acq On 15 Apr 2002 10:43 am Operator: Nefliu Sample Inst Instrume Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Abundance TIC: DFTPP1.D 1500000

1000000

500000

Time-> o' Abundance 16 00 A 16 50 17 00 17.50 A 18 00 — 18.50 19.00 19.50 Average of 17.745 to 17 756 min DFTPP 1 D 198 442 150000

100000 255 127 77 51 50000 110 275 224 296 , 423

n/Z-> 0 AL4 40 60 80 93 1 148 167180 i -++++ 41144.24,, Tmmmmnt _ I 323 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440 352365 383 403

Spectrum Information: Average of 17.745 to 17.756 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 31.4 53720 PASS 68 69 0.00 2 1.4 822 PASS 69 198 0.00 100 34.1 58328 PASS 70 69 0.00 2 0.5 268 PASS 127 198 40 60 46.5 79440 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 170858 PASS 199 198 5 9 6.8 11595 PASS 275 198 10 30 24.3 41549 PASS 365 198 1 99 3.4 5765 PASS 441 443 1 100 83.6 26066 PASS 442 198 40 110 93.7 160074 PASS 443 442 17 23 19.5 31173 PASS

DFTPP1.D 041202SCAN.M Wed Apr 17 15:54:26 2002

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