GCMS analysis results, sample AE07512, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07512.D Vial: 8 Acq On 4 Apr 2002 1:30 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 Krypton Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 3.26 0.12 ug/1 65389 1,4-Dichlorobenzene-d4 10.65 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Krypton 84 Kr 007439-90-9 2 2 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17-0 2 3 2-Methyl-3-vinyl-oxirane 84 C5H80 006790-37-0 1 4 2-Chloroethanol 80 C2H5C10 000107-07-3 1 Abundance Scan 30 (3.256 min): 07512. D (-21) (-) m/z 84.00 100.00% 40 . 84

5000

40 3.20 3.30 3.40 3.50 3.60 3.70 Oh TTTT ' i ■ ■ ■ ■ i ■ ■1 ■ i ■'111 ■ ■ ■ ■ i ■'' ■ i'r ■ ■ । ■ ■ ■ ■ ।1 m/z 49.10 99.45% m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33829: Krypton 84

5000 3.20 3.30 3 40 3.50 3.60 3.70 42 m/z 86.00 84.45%

n/z-> oh 15 Abundance 1141**1*11′1′71111 20 25 30 35 > > 1111 ■ i • > • • । 40 ■ i • ■' • । ■ 45 50 55 60 65 70 #34862: Imidazol, 4-fluoro- ■ I > < i11 ■ । ■ 11 ■ ■ t11 ■

75 80

80 85 > > i • ■ ■ ■ i ■ 90 95 .MMWnug, 85

3.20 3.30 3.40 3.50 3.60 3.70 5000 m/ Z 47.00 69.24%

Oh 59 ■ ■ i ■ ■ > ■ i ■ ■ ■ ■ i ■ ■ ■ ■ l ■ ■ ■ ■ i —Imm , J. n/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1297: 2-Methyl-3-vinyl-oxirane ■' i' •1' i ■ ■ ■ ■ i ■

39 55 3.20 3.30 3.40 3.50 3.60 3.70 m/z 51.00 43.77%

5000 27 45

69 83 /MMvat Oh T’IT —12136 —42 48 51 , 11111111 F8,60 63"■6566I111170,!"1 7577 80 +9—7PPP 11 ■ ■ ’ ■ i I'' ' 1 I ' ' ' ' I i' ■'' i '' ■ ■ i ■' n/z-> 15 20 25 30 35 40 45 50 55 85 90 95 3.20 3.30 3.40 3.50 3.60 3.70

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