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Document / 11 pages

GCMS analysis report, sample AE07569, April 2002

Machine-extracted title · confidence 100%

Laboratory results for unknown compounds and surrogate recovery in sample AE07569 analyzed on April 9, 2002.

NYC-WTC_000047216–000047226

Folder label: “GCMS X 4/2/02 A 4/3/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020403\07569.D Vial: 17 Acq On 3 Apr 2002 11:52 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 04 08:14:51 2002 Quant Results File: SCAN020403 .RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Thu Apr 04 08:10:12 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 10.66 152 2743064 20.00 ug/1 0.00 10) Naphthalene-d8 15.77 136 10062717 20.00 ug/1 0.00 17) Acenaphthene-dlO 23.66 164 5790331 20.00 ug/1 -0.01 31) Phenanthrene-dlO 30.89 188 9425240 20.00 ug/1 0.00 39) Chrysene-dl2 39.09 240 7228513 20.00 ug/1 -0.02 45) Perylene-dl2 42.30 264 3928306 20.00 ug/1 -0.01 System Monitoring Compounds 2 8) TCMX 26.72 207 207729 3.67 ug/1 / 0.00 Spiked Amount 5.000 Recovery = 73.40% ( 200 Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 07569.D SCAN020403 ,M Thu Apr 04 10:58:00 2002 Page 1

NYC-WTC_000047218

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NYC-WTC_000047218Source: NYC Law Department, mirrored locally

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