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Document / 11 pages

GCMS method file details for April 3-5, 2002

Machine-extracted title · confidence 90%

Technical documentation listing GC/MS method parameters and internal standard data for analysis performed in early April 2002.

NYC-WTC_000047452–000047462

Folder label: “GCMS X 4/3/02 A 4/5/02

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OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\020404\07767.D Vial: 21 Acq On 5 Apr 2002 1:34 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 05 14:31:26 2002 Quant Results File: SCAN020403.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Fri Apr 05 14:03:06 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 10.66 152 2644536 . 20.00 ug/1 0.00 10) Naphthalene-d8 15.77 136 9754901 20.00 ug/1 0.00 17) Acenaphthene-diO 23.66 164 5626287 20.00 ug/1 -0.01 31) Phenanthrene-dlO 30.90 188 9215552 20.00 ug/1 0.00 39) Chrysene-dl2 39.10 240 7365457 20.00 ug/1 -0.01 45) Perylene-dl2 42.30 264 3935429 20.00 ug/1 0.00 System Monitoring Compounds 2 8) TCMX _ 26.73 207 447651 8.13 ug/1_ 0.00 Spiked Amount 4.000 Recovery = 203.25% Target Compounds 0 /0~ Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 07767.D SCAN020403.M Fri Apr 05 14:31:41 2002 Page 1

NYC-WTC_000047454

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NYC-WTC_000047454Source: NYC Law Department, mirrored locally

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