GCMS results for sample AE07766, Apr 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\07766.D Vial: 28 Acq On : 16 Apr 2002 8:51 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 9 Furan, 2,5-dihydro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

29.31 0.41 ug/L 409115 Chrysene-dl2 30.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Furan, 2,5-dihydro- 70 C4H60 001708-29-8 9 2 2-Propyn-1-amine, N,N-dimethyl- 83 C5H9N 007223-38-3 9 3 2-Pentanol, 5-(2-propynyloxy) - 142 C8H14O2 055702-67-5 9 4 Methanesulfonic acid, pentyl ester 166 C6H14O3S 006968-20-3 9 Abundance Scan 4464 (29.308 min)' 07766.D (-4462) (-) m/z 10 9.30 100.00% 109 70 85 42 49 57 5000 95 29 00 29 20 2940 29.60 0+ ■ 1 i ■ 1 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i m/z 85.30 79.30% Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance 4h #108474 Furan. 2,5-dihydro- 70 mhA"M/WA 5000- t 1 ■ ■ ■ i 1 1 1 29.00 29.20 2940 29.60 29 m/z 42.30 74.89%

n/z--> 0+ ...... .d.. I I, m- 10 50 ......... -4 20 30 40 50 60 :70 80 + --------- 90 110 120 130 100 Abundance #3554: 2-Propyn-1-amme, N,N-dimethyl- 42 82

29.00 29 20 29.40 29 60 5000 m/z82.40 74.89% 58 A 15 28 67

n/z— > 0 10 f 20 ++30 3fiih1 40 ,52,1 50 60 70 80 1 ' 90" ' ' l66 110 120 130 A

Abundance #1282: 2-Pentanol. 5-(2-propynyloxy) 4 39 29.00 29.20 29 40 29.60 45 m/ z 70.30 74.45% 5000 29 71 55 85 15

n/z-> 0 —4 10 20 +H 50 — 60 — 65111 70 — 79 14- 80 91 98 104 112 <90 123 1 1 1 ,,rl l 1"1 1 1 1 1 ' ‘ ' I ' 1 1 1 1 1 100 110 120 130 ) 29 00 29.20 29.40 29 60

07766.D 041202SCAN.M Tue Apr 16 13:42:11 2002 Page 12

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