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GCMS analysis results for sample AE08066, Apr 2002

Machine-extracted title · confidence 100%

Laboratory report documenting the GCMS analysis of sample AE08066 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046786–000046798

Folder label: “GCMS X 4/5/02 A 4/16/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020415\08066.D Vial 23 Acq On 16 Apr 2002 4:47 am Operator Nefliu Sample sample Inst Instrumen Mise Multiplr 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 16 13:54:49 2002 Quant Results File: 041202SCAN.RE

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Last Update Tue Apr 16 11:14:47 2002 Response via Initial Calibration DataAcq Meth 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.99 152 4936619 40.00 ug/L 0.00 10) Napthalene-d8 13.48 136 18693992 40.00 ug/L -0.01 17) Acenapthalene-dlO 18.63 164 10950388 40.00 ug/L -0.01 29) Phenanthranene-dlO 23.02 188 16819273 40.00 ug/L -0.01 37) Chrysene-dl2 30.88 240 12576834 40.00 ug/L -0.02 43) Perylene-dl2 34.78 264 7896308 40.00 ug/L -0.02

System Monitoring Compounds 2 7) TCMX 20.60 207 380299 6.26 ug/L 0.00 Spiked Amount 8.000 Recovery = 78.25%

Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08066.D 041202SCAN.M Tue Apr 16 13:55:34 2002 Page 1

NYC-WTC_000046788

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NYC-WTC_000046788Source: NYC Law Department, mirrored locally

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