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GCMS analysis results for sample AE07312, April 2002

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Laboratory report documenting GCMS analysis of sample AE07312 conducted on April 10, 2002, including surrogate recovery data.

NYC-WTC_000046613–000046623

Folder label: “GCMS X 3/28/02 A 2/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR0302\7312.D Vial: 8 Acq On 3 Apr 2002 7:35 pm Operator: Sample gc/ms scan 3/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 8 11:48 2002 Quant Results File: GCMS0403.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Apr 08 11:30:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Compound R.T. Qlon Response Cone Unit Qvalue

27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.63 178 354 N.D. 35) Anthracene 25.63 178 354 N.D. 36) Di-n-butylphthalate 27.60 149 8951 N.D. 37) Fluoranthene 0.00 202 0 N.D. 40) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 32.13 149 198 N.D. 42) Benzo(a)anthracene 33.69 228 1522 N.D. 43) Bis(2-ethylhexyl)phthalate 33.90 149 84721 4.49 ug/1 98 44) Chrysene 33.77 228 189 N.D. 46) Di-n-Octylphthalate 0.00 149 0 N.D. 47) Benzo(b)fluoranthene 36.76 252 401 N.D. 48) Benzo(k)fluoranthene 36.81 252 718 N.D. 49) Benzo(a)pyrene 37.93 252 1238 N.D. 50) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 7312 .D GCMS0403.M Mon Apr 08 11:49:20 2002 Page 2

NYC-WTC_000046616

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NYC-WTC_000046616Source: NYC Law Department, mirrored locally

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