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GCMS calibration results for sample AE07311, April 2002

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Laboratory report displaying GCMS calibration data for sample AE07311 conducted on April 3, 2002.

NYC-WTC_000046554–000046565

Folder label: “GCMS X 3/28/02 A 2/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR0302\LB.D Vial: 3 Acq On 3 Apr 2002 1:38 pm Operator: Sample gc/ms scan 3/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 8 11:31 2002 Quant Results File: GCMS0403.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Apr 08 11:30:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Compound R.T. Qlon Response Cone Unit Qvalue

27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.70 178 318 N.D. 35) Anthracene 25.70 178 318 N.D. 36) Di-n-butylphthalate 27.60 149 8262 N.D. 37) Fluoranthene 29.33 202 213 N.D. 40) Pyrene 29.99 202 590 N.D. 41) Butylbenzylphthalate 32.13 149 511 N.D. 42) Benzo(a)anthracene 33.68 228 4381 N.D. 43) Bis(2-ethylhexyl)phthalate 33.91 149 72960 4.19 ug/1 100 44) Chrysene 33.63 228 2389 N.D. 46) Di-n-Octylphthalate 35.64 149 681 N.D. 47) Benzo(b)fluoranthene 36.75 252 1233 N.D. 48) Benzo(k)fluoranthene 36.82 252 1614 N.D. 49) Benzo(a)pyrene 37.74 252 816 N.D. 50) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i )perylene 43.31 276 813 N.D.

(#) = qualifier out of range (m) = manual integration LB.D GCMS0403.M Mon Apr 08 11:32:27 2002 Page 2

NYC-WTC_000046556

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NYC-WTC_000046556Source: NYC Law Department, mirrored locally

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