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GCMS calibration results for sample AE07311, April 2002

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Laboratory report displaying GCMS calibration data for sample AE07311 conducted on April 3, 2002.

NYC-WTC_000046554–000046565

Folder label: “GCMS X 3/28/02 A 2/27/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APRO3O2\LB.D Vial: 3 Acq On 3 Apr 2002 1:38 pm Operator: Sample gc/ms scan 3/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K. L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.85 1.65 ug/1 244514 Naphthalene-d8 15.88

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6(83 2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 3 Phenethylamine, N-methyl-.beta. , 3,4 399 C18H37NO3Si3 010538-85-9 38 4 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 38 Abundance Scan 1068 (14.847 min): LB.D (-) m/z 73.00 100.00% 73

5000 267 355

■ 1 i 1 1 y............ ■ ■ ■ I ■ 1 ' 1 I 1 ■

45 14.60 14.80 15.00 15.20 103118133 154 177 193208223 251 293 323339 uiatlli I’*III’ISII " '' 'l'' I' I 111'1' " I'11 ‘ I (l t ToTis rT . m/z 2 67.00 46.65% /z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 — 5000 14.60 14.80 15.00 15.20 m/z 355.05 46.03% i-i-p i ■ ■11 191207 323339 TTT I’I r ' ■ ■ i ‘1 ■ ' i 251 1 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 \ । ‘ । * 1 14.60 14.80 15.00 15.20 267 m/z 3 56.05 16.45% 5000 179 356 45 147 |, 209 237 , 312 341 rp-r mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 14.60 14.80 15.00 15.20 m/z 2 68.00 11.39%

5000 355 44

m/z—> L —188— 11 ‘11 ■1 ■11 130147 i' 1’fi ] ।11111' 11 193 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 267 294 ph .............. \.................. ' 1 i ' ■ 1 ■ i 1 ■ 1 1 I 1 1 1 1 I 1 ' 14.60 14.80 15.00 15.20

LB.D GCMS0403.M Tue Apr 09 13:09:22 2002 Page 2

NYC-WTC_000046561

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NYC-WTC_000046561Source: NYC Law Department, mirrored locally

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