NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\APRO3O2\LB.D Vial: 3
Acq On 3 Apr 2002 1:38 pm Operator:
Sample gc/ms scan 3/28 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator)
Title 209 625/TCLP calibration table
Library C:\DATABASE\NBS75K. L
*********************************************************************
Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
14.85 1.65 ug/1 244514 Naphthalene-d8 15.88
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6(83
2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43
3 Phenethylamine, N-methyl-.beta. , 3,4 399 C18H37NO3Si3 010538-85-9 38
4 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 38
Abundance Scan 1068 (14.847 min): LB.D (-) m/z 73.00 100.00%
73
5000 267 355
■ 1 i 1 1
y............
■ ■ ■ I ■ 1 ' 1 I 1 ■
45 14.60 14.80 15.00 15.20
103118133 154 177 193208223 251 293 323339
uiatlli I’*III’ISII " '' 'l'' I' I 111'1' " I'11 ‘ I (l t ToTis rT . m/z 2 67.00 46.65%
/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267 —
5000
14.60 14.80 15.00 15.20
m/z 355.05 46.03%
i-i-p i ■ ■11
191207 323339
TTT I’I
r ' ■ ■ i ‘1 ■ ' i
251 1
n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)-
73
\ । ‘ । * 1
14.60 14.80 15.00 15.20
267 m/z 3 56.05 16.45%
5000 179
356
45 147
|, 209 237 , 312 341
rp-r
mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls
73 14.60 14.80 15.00 15.20
m/z 2 68.00 11.39%
5000 355
44
m/z—>
L —188— 11 ‘11 ■1 ■11
130147
i' 1’fi ] ।11111' 11
193
40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
267 294
ph .............. \..................
' 1 i ' ■ 1 ■ i 1 ■ 1 1 I 1 1 1 1 I 1 '
14.60 14.80 15.00 15.20
LB.D GCMS0403.M Tue Apr 09 13:09:22 2002 Page 2
NYC-WTC_000046561
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