GCMS analysis results for sample AE09156, May 2002

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Data File : C:\MSDCHEM\1\DATA\020424\09153.D Vial: 22 Acq On : 25 Apr 2002 6:29 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.349 38 46 57 PV 3 15339 273078 0.34% 0.061% 2 3.649 93 97 105 PV 3 22196 313624 0.39% 0.070% 3 6.123 510 518 520 PV 2 60548 1294986 1.61% 0.289% 4 6.158 520 524 569 W 1002194 20233333 25.12% 4.520% 5 11.375 1401 1412 1431 PV 2093752 50908984 63.21% 11.373%

6 15.465 2093 2108 2132 PV 224871 6525679 8.10% 1.458% 7 16.534 2272 2290 2306 PV 2698974 70378641 87.38% 15.722% 8 24.460 3615 3639 3655 PV 2985251 80540214 100.00% 17.992% 9 27.539 4148 4163 4177 PV 271228 7394313 9.18% 1.652% 10 31.094 4758 4768 4778 W 4 20020 620299 0.77% 0.139%

11 31.723 4857 4875 4893 W 2 2704306 79068430 98.17% 17.663% 12 31.952 4905 4914 4924 W 2 21688 612074 0.76% 0.137% 13 39.937 6258 6273 6292 PV 2 3834716 72086873 89.50% 16.104% 14 40.524 6367 6373 6382 PV 3 24607 569535 0.71% 0.127% 15 43.156 6810 6821 6839 PV 2 2846435 56826070 70.56% 12.694%

Sum of corrected areas: 447646132

09153.D SCAN020424.M Fri May 03 11:00:15 2002 Page 1

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