GCMS analysis results for sample AE08959, May 7, 2002

NYC 9/11 Public Portal Document

'Data File : C:\MSDCHEM\1\DATA\020424\08959.D Vial: 10 Acq On : 24 Apr 2002 6:43 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.350 43 46 50 W 4 18709 211857 0.26% 0.048% 2 3.649 93 97 107 W 3 15655 277584 0.34% 0.063% 3 6.152 512 523 543 PV 875383 15994650 19.73% 3.627% 4 6.276 543 544 550 VB 5 12239 168464 0.21% 0.038% 5 11.376 1399 1412 1432 PV 2072966 51575157 63.61% 11.697% 6 16.534 2267 2290 2307 PV 2708468 71502674 88.19% 16.216% 7 24.461 3617 3639 3652 PV 2898058 81078578 100.00% 18.388% 8 24.619 3657 3666 3675 W 4 16158 446260 0.55% 0.101% 9 27.539 4150 4163 4174 PV 2 319552 8977359 11.07% 2.036% 10 31.088 4759 4767 4777 W 3 19731 629292 0.78% 0.143% 11 31.717 4854 4874 4893 W 2 2684793 79838964 98.47% 18.106% 12 31.958 4908 4915 4924 W 2 21055 554943 0.68% 0.126% 13 39.937 6262 6273 6287 PV 3943099 72872837 89.88% 16.527% 14 43.157 6805 6821 6841 PV 2958465 56815065 70.07% 12.885%

Sum of corrected areas: 440943685

08959.D SCAN020424.M Thu May 02 14:41:09 2002 Page 1

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