GCMS calibration results for sample AE09152, April 2002

z Z K Quantitation Report (QT Reviewed) K o o 3 Data File : C:\MSDCHEM\1\DATA\020424\0424C3.D Vial: 2 CD — o Acq On : 24 Apr 2002 9:57 am Operator: Nefliu "0 I o Sample : CCV Inst Instrumen C O o o o Mise Multiplr: 1.00 o' MS Integration Params: EVENTS.E "0 o) o CD Quant Time: Apr 24 10:45 2002 Quant Results File: SCANO20424.RES — CD O. 0 O Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) o Q C Title : Method 508 GC/MS Scan 3 Last Update : Wed Apr 24 08:54:34 2002 CD X Response via : Initial Calibration Abundance TIC: 0424C3.D 6000000

5500000 g1 ® TO

2o £ it g 2

J TO 5000000 2 2 g 1i !6 g2 8 i TO

ill 8> i i o g

I 2 (o 2 % i § CM w 4500000 £ £ 1 1 s 83 E g 8 C ill s5 8 2 z 2a 18 2 105 88 88 4000000 TO £ 2 2 J & 6 85 Qo o2 2 TO & TO

| S 1s5 c 3500000 If Z e| 5 fE a $8 § 2 g 89 1 CM & 3000000 ill Q 122 CD 6 f& N

1

i 8 3 g&a $2e 2- 2 | 3 3 11 s a

8 99 2 2 II 3 f a S

5 I 2500000 Iw 86 188 « 8 2 ro 8 X ! z 2 82 52 2000000 2 2 gk z 1 8

1500000

1000000 tI & CM* CM

y3 500000

0 a JLL —L U li Ml I L T"r Time-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 40.00 42.00 44.00

0424C3.D SCAN020424.M Wed Apr 24 10:45:49 2002 Page 3