Gas chromatography-mass spectrometry analysis of sample AE10808 performed May 17, 2002, including unknown compound detection and surrogate recovery testing.
NYC-WTC_000046372–000046381Folder label: “GCMS X 5/7/02 A 5/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\MAY0802\10808.D Vial: 23 Acq On 9 May 2002 8:08 am Operator : Sample GC/MS SCAN 5/7 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 10 8:19 2002 Quant Results File: GCMS0507.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu May 09 14:27:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.19 152 433202 40.00 ug/1 0.00 10) Naphthalene-d8 15.83 136 1588838 40.00 ug/1 0.00 17) Acenaphthene-diO 21.13 164 867527 40.00 ug/1 0.00 30) Phenanthrene-diO 25.58 188 1188314 40.00 ug/1 0.00 38) Chrysene-dl2 33.63 240 740501 40.00 ug/1 0.00 44) Perylene-dl2 37.86 264 449362 40.00 ug/1 0.00
System Monitoring Compounds 28) TCMX 23.27 209 39170 9.08 ug/L 0.00 Spiked Amount 10.000 Recovery = 90.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(l-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.88 128 196 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.62 149 1267 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.58 178 223 N.D.
(#) = qualifier out of range (m) = manual integration 10808.D GCMS0507.M Fri May 10 08:19:51 2002 Page 1
NYC-WTC_000046374
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NYC-WTC_000045849
Gas chromatography-mass spectrometry reference report for sample AE10772 listing measured values and detection limits.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045859
Gas chromatography-mass spectrometry report for sample AE10773 showing detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046360
Laboratory report documenting GCMS analysis of sample AE10807 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023353
Laboratory report showing GC/MS analysis results for sample AE09520 including surrogate recovery data on May 16, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023316
Laboratory report showing GC/MS analysis results for sample AE09578 including surrogate recovery data on May 16, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023273
Laboratory report showing GCMS analysis of sample AE08485 conducted on May 16, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023635
Gas chromatography-mass spectrometry analysis of sample AE09398 conducted May 15, 2002, with surrogate 2,4-DDD recovery at 79 percent.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047734
Laboratory report documenting GCMS analysis of sample AE08019 conducted on April 24, 2002, including surrogate recovery data.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038861
Laboratory report documenting GCMS analysis of sample AE02576 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049147
Laboratory report documenting GCMS analysis of sample AE08834 conducted on April 25, 2002, showing detection of unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012710
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11597.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000040088
Laboratory report documenting GCMS analysis of environmental sample AE06997 conducted on April 16, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000046213
Department of Environmental Protection GCMS analysis record for the World Trade Center site dated May 7-9 2002.
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NYC-WTC_000046214
Single page excerpt from a GCMS laboratory record file stored in DEP Box 25, dated between May 7 and May 9, 2002.
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NYC-WTC_000046217
Laboratory data sheet recording GCMS blank analysis parameters for sample AE09579 conducted on May 8, 2002.
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NYC-WTC_000046226
Laboratory report of GCMS calibration analysis for sample AE09579 conducted on May 8, 2002, listing detection limits.
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NYC-WTC_000046230
Laboratory report of GCMS reference analysis for sample AE09579 conducted on May 8, 2002, showing response factors.
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