GCMS analysis results for sample AE10608, May 2002

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Laboratory report documenting GCMS analysis of sample AE10608 including surrogate recovery data conducted on May 15, 2002.

NYC-WTC_000045434–000045442

Folder label: “GCMS X 5/3/02 A 5/8/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0802\10608.D Vial: 7 Acq On 8 May 2002 4:26 pm Operator: Sample GC/MS SCAN 5/3 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 9 14:35 2002 Quant Results File: GCMS0507.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0507. M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu May 09 14:27:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 461738 40.00 ug/1 0.00 10) Naphthalene-d8 15.83 136 1664054 40.00 ug/1 0.00 17) Acenaphthene-dlO 21.13 164 901338m 40.00 ug/1 0.00 30) Phenanthrene-diO 25.58 188 1206987 40.00 ug/1 0.00 38) Chrysene-dl2 33.63 240 596118 40.00 ug/1 0.00 44) Perylene-dl2 37.86 264 352363 40.00 ug/1 0.00

System Monitoring Compounds 2 8) TCMX 23.27 209 37308m 8.32 ug/L 0.00 Spiked Amount 10.000 Recovery = 83.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.88 128 755 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.62 149 880 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.63 178 925 N.D.

(#) = qualifier out of range (m) = manual integration 10608.D GCMS0507.M Thu May 09 14:35:18 2002 Page 1

NYC-WTC_000045436

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GCMS analysis results, sample AE06048, May 6, 2002 · Box DEP Box 25

NYC-WTC_000043220

Laboratory report for DEP Box 25 showing GCMS analysis of sample AE06048 with unknown compounds and surrogate data from May 6, 2002.

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