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GCMS sample analysis results for unknowns, May 2002

Machine-extracted title · confidence 95%

Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10132 on May 17, 2002.

NYC-WTC_000046147–000046158

Folder label: “GCMS X 5/7/02 A 5/14/02

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Scanned page image, NYC-WTC_000046149
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020513\10132.D Vial: 19 Acq On : 14 May 2002 6:22 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 14 16:00:25 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 465261 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1747558 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 928242 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1577885 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1247856 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 768835 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.54 207 71586m 9.65 ug/1 -0.04 Spiked Amount 10.000 Recovery = 96.50%

Target Compounds Qvalue 29) Azobenzene 28.10 77 67 0.00 ug/1 61 43) Bis(2-ethylhexyl )phthalate 40.52 149 5224 0.20 ug/1 95

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10132.D SCAN020507.M Wed May 15 09:54:17 2002 Page 1

NYC-WTC_000046149

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NYC-WTC_000046149Source: NYC Law Department, mirrored locally

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