GCMS Method 06 header page, May 2002

NYC 9/11 Public Portal Document

DFTPP

Data File C:\MSDCHEM\1\DATA\020513\DFTPP.D Vial: 1 Acq On 13 May 2002 12:46 pm Operator: Nefliu Sample Inst : Instrume Mise : Multiplr: 1.00 MS Integration Params: rteint.e Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan

Abundance TIC: DFTPP.D

4000000

3000000

2000000

1000000

o’ . i . Time-> 16.00 16.50 17.00 17.50 18.00 18.50 19.00 19.50 Abundance Average of 17.813 to 17.836 min.: DFTPP.D 198

300000 442

255 200000 51 77 127

110 100000 275 224

226 323 , 346 365 383 403 423 /z-> 37 0 ■ ■ ■111' — 40 60 80 448 17181.4.1,24., LX — ————————— 1rT 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Average of 17.813 to 17.836 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 53.7 188848 PASS 68 69 0.00 2 1.7 2830 PASS 69 198 0.00 100 47.1 165781 PASS 70 69 0.00 2 0.4 746 PASS 127 198 40 60 51.0 179557 PASS 197 198 0.00 1 0.3 950 PASS 198 198 100 100 100.0 351893 PASS 199 198 5 9 6.6 23109 PASS 275 198 10 30 24.1 84813 PASS 365 198 1 99 3.3 11715 PASS 441 443 1 100 81.7 43842 PASS 442 198 40 110 83.1 292330 PASS 443 442 17 23 18.4 53664 PASS

DFTPP.D SCAN020507.M Wed May 15 09:12:04 2002

NYC-WTC_000046116