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GCMS analysis results for sample AE10811, May 2002

Machine-extracted title · confidence 50%

Gas chromatography-mass spectrometry report for sample AE10811 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000046036–000046063

Folder label: “GCMS X 5/7/02 A 5/15/02

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NYC 9/11 Public Portal Document

Operator ID: Mclean Date Acquired: 15 May 2002 6:39 am Data File: C:\MSDCHEM\l\DATA\051402\10811.D Name: 5/7 kb Mise: Method: C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title: 508 Modified GC/MS scan Library Searched: C:\DATABASE\NIST98.L

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone

Methane, bromodic... 3.34 0.2 ug/L 214777 1 9.94 37645900 40.0 Acetonitrile, die... 3.62 0.5 ug/L 469078 1 9.94 37645900 40.0 Acetyl chloride 3.75 0.3 ug/L 308879 1 9.94 37645900 40.0 1,3,5-Triazine-2,... 5.10 0.2 ug/L 209603 1 9.94 37645900 40.0 2-Pentanone, 4-hy... 5.97 14.3 ug/L 13501100 1 9.94 37645900 40.0 3-Oxetanol, 2,2,3... 7.73 0.3 ug/L 311716 1 9.94 37645900 40.0 Cyclotetrasiloxan... 9.25 0.8 ug/L 761362 1 9.94 37645900 40.0 Cyclopentasiloxan ... 12.41 1.9 ug/L 2389490 2 13.43 50563600 40.0 Benzaldehyde, ethyl- 14.04 0.2 ug/L 301442 2 13.43 50563600 40.0 Cyclohexasiloxane. .. 15.48 2.3 ug/L 2849740 2 13.43 50563600 40.0 Cycloheptasiloxan... 18.23 1.3 ug/L 1720060 3 18.57 54676500 40.0 Benzoic acid, 4-e... 19.19 0.5 ug/L 741170 3 18.57 54676500 40.0 Phenethylamine , N... 20.68 0.8 ug/L 1056450 3 18.57 54676500 40.0 Phenanthrene, 9-m... 22.58 0.3 ug/L 394160 4 22.95 52380100 40.0 1,1,1,5,7,7,7-Hep... 22.80 0.5 ug/L 596986 4 22.95 52380100 40.0 Benzene, l-(l-cyc... 23.11 0.5 ug/L 628249 4 22.95 52380100 40.0 Trisiloxane, 1,1,... 24.68 0.2 ug/L 290684 4 22.95 52380100 40.0 Pyrazolo[1,5-a]py... 36.48 0.4 ug/L 296270 6 34.70 32061600 40.0

10811.D 050102.M Thu May 16 14:13:36 2002 Page 23

NYC-WTC_000046063

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NYC-WTC_000046063Source: NYC Law Department, mirrored locally

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