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GCMS blank analysis results, sample AE10809, May 2002

Machine-extracted title · confidence 80%

Gas chromatography-mass spectrometry blank analysis conducted May 17, 2002 testing for semivolatile organic compounds with all results below method reporting limits.

NYC-WTC_000045936–000045963

Folder label: “GCMS X 5/7/02 A 5/15/02

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NYC 9/11 Public Portal Document

Operator ID: Mclean Date Acquired: 15 May 2002 2:34 am Data File: C:\MSDCHEM\1\DATA\051402\0507LB.D Name: 5/7 kb Mise: Method: C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title: 508 Modified GC/MS scan Library Searched: C:\DATABASE\NIST98.L

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone

Diethylpropion Hy.. 3.82 0.3 ug/L 233168 1 9.93 27176600 40.0 Cyclotrisiloxane,.. 5.40 0.4 ug/L 237950 1 9.93 27176600 40.0 2-Pentanone, 4-hy.. 5.96 11.8 ug/L 8008080 1 9.93 27176600 40.0 Cyclotetrasiloxan .. 9.25 1.6 ug/L 1077520 1 9.93 27176600 40.0 Cyclopentasiloxan .. 12.41 2.7 ug/L 2449700 2 13.43 36137200 40.0 Cyclohexasiloxane. . 15.48 2.9 ug/L 2640020 2 13.43 36137200 40.0 Cycloheptasiloxan .. 18.23 1.6 ug/L 1521220 3 18.56 38739700 40.0 Benzoic acid, 4-e.. 19.19 0.6 ug/L 559852 3 18.56 38739700 40.0 Benzoic acid, 2,6.. 20.68 0.9 ug/L 825203 3 18.56 38739700 40.0 1,1,1,5,7,7,7-Hep. . 22.80 0.5 ug/L 412664 4 22.95 35663000 40.0 Anthracene-dlO- 23.11 0.3 ug/L 303537 4 22.95 35663000 40.0 3,6-Dioxa-2,4,5,7. . 33.10 2.7 ug/L 1218230 6 34.70 18222200 40.0 Plumbane, triethy.. 33.17 1.1 ug/L 484009 6 34.70 18222200 40.0 Butanoic acid, 3-.. 33.23 0.7 ug/L 335227 6 34.70 18222200 40.0 2-t-Butyl-6-(2-hy.. 34.88 0.4 ug/L 183591 6 34.70 18222200 40.0 3-Benzofurancarbo.. 35.42 0.3 ug/L 140911 6 34.70 18222200 40.0 1,1,1,5,7,7,7-Hep. . 36.45 2.6 ug/L 1197160 6 34.70 18222200 40.0 2-Propenoic acid,.. 36.48 2.1 ug/L 966113 6 34.70 18222200 40.0 .alpha.-Tetraloxi.. 37.77 0.3 ug/L 136852 6 34.70 18222200 40.0 3,6-Dioxa-2,4,5,7.. 39.76 2.7 ug/L 1232100 6 34.70 18222200 40.0

0507LB.D 050102.M Thu May 16 12:36:05 2002 Page 24

NYC-WTC_000045963

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NYC-WTC_000045963Source: NYC Law Department, mirrored locally

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