GCMS analysis results for sample AE10810, May 2002

NYC 9/11 Public Portal Document

•Data File : C:\MSDCHEM\1\DATA\051402\10810.D Vial : 20 Acq On : 15 May 2002 5:50 am Operator: Mclean Sample : 5/7 kb Inst : Instrumen Miso : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C : \DATABASE\NIST98 . L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

3.62 0.39 ug/L 365460 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 74 2 Allyl mercaptan 74 C3H6S 000870-23-5 9 3 Thiirane, methyl- 74 C3H6S 001072-43-1 5 4 Furan, 2-methyl- 82 C5H60 000534-22-5 5 Abundance Scan 93 (3.626 min): 10810.D (-87) (-) m/ z 74.00 100.00% 7|4

82 5000 47 38 3.20 3.40 3.60 3.80 4.00 Of 1 I ' ' 1 ' I ' . 1 14 58 1 I ' 11 1 1 1 1 ' m/z 82.00 54.42% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338 Acetonitrile, dichloro- 74

5000 82 I"1 ‘ 1 1 NA l r । ’'"I | I-' a < i | i i > i | i । i

3.20 3.40 3.60 3.80 4.00 47 m/z 84.00 28.86% 35

m/z-> Of

Abundance II 10 12 26 | i 1 1 | 1 1,1,1 1 1 1 1 ' r1 20 30 40 , JH|,,, 62-— 50 60 70 #28161: Allyl mercaptan 80 | I I p I

90 I F I

100 | I I 108 I I

110 | I I * 1 | MWs/ulu 41 74 i ' ' ' 1 1 1 ' ' 1 I ' 3.20 3.40 3.60 3.80 4.00 5000 m/z 76.00 27.78% 1 47 0! 27 33 J , 11, 53 59,68,1 ................. -I1' 1 1a1/1— 1—r 11—I—1—I 11*1 I I I 1 * 1 '' 1 i ■ 1 1 1 i 1 ' 1 1 i 1 1 ' 1 I 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115343: Thiirane, methyl- ----- kik 41 74 3.20 3.40 3.60 3.80 4.00 m/ z 47.05 23.12%

5000

47 aMWwp MMWAoW + 1,53 59 68,,1 11 .......... . ............... , 27 33 , ------ 0 1 I [ m i t । । i r f [ r

m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80 4 00

10810.D 050102.M Thu May 16 12:39:17 2002 Page 5

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