GCMS analysis results for sample AE10809, May 2002

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Gas chromatography-mass spectrometry report for sample AE10809 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000045984–000046005

Folder label: “GCMS X 5/7/02 A 5/15/02”

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NYC 9/11 Public Portal Document 40 11.863 1487 1495 1499 PV 4 4820 79899 0.12% 0.021%

41 12.040 1519 1525 1538 PV 2 4494 93634 0.14% 0.024% 42 12.410 1577 1588 1595 W 26806 438197 0.63% 0.113% 43 12.527 1595 1608 1613 W 7 2417 65941 0.10% 0.017% 44 12.662 1613 1631 1636 W 7 1899 49604 0.07% 0.013% 45 12.721 1636 1641 1648 W 2743 55681 0.08% 0.014%

46 12.903 1664 1672 1679 W 4 1981 52143 0.08% 0.013% 47 13.197 1717 1722 1729 W 4 1925 42084 0.06% 0.011% 48 13.432 1752 1762 1779 PV 3302757 64084943 92.54% 16.535% 49 13.579 1779 1787 1797 W 12933 257631 0.37% 0.066% 50 13.826 1823 1829 1839 W 5 5902 116571 0.17% 0.030%

51 14.043 1855 1866 1877 W 5 3890 92273 0.13% 0.024% 52 14.607 1956 1962 1968 W 3 1714 31756 0.05% 0.008% 53 15.483 2100 2111 2123 PV 24964 429994 0.62% 0.111% 54 15.700 2132 2148 2156 W 4 3793 109010 0.16% 0.028% 55 15.900 2171 2182 2192 W 2 2652 62484 0.09% 0.016%

56 16.746 2319 2326 2340 W 6 7201 183762 0.27% 0.047% 57 17.145 2390 2394 2400 W 4 2695 40475 0.06% 0.010% 58 18.232 2567 2579 2591 PV 28356 467857 0.68% 0.121% 59 18.573 2626 2637 2663 W 3382023 69251185 100.00% 17.868% 60 18.961 2692 2703 2716 W 4 2930 79134 0.11% 0.020%

61 19.184 2737 2741 2760 W 2 4272 86608 0.13% 0.022% 62 20.142 2900 2904 2917 W 4 3064 63227 0.09% 0.016% 63 20.324 2927 2935 2943 VB 4 2424 44368 0.06% 0.011% 64 20.536 2961 2971 2984 PV 616136 11227946 16.21% 2.897% 65 20.683 2989 2996 3019 W 24072 415356 0.60% 0.107%

66 21.393 3112 3117 3124 W 3 3792 61513 0.09% 0.016% 67 21.758 3165 3179 3183 PV 4 4185 74303 0.11% 0.019% 68 22.580 3311 3319 3329 W 2 31039 566820 0.82% 0.146% 69 22.798 3348 3356 3364 PV 2 12743 219879 0.32% 0.057% 70 22.956 3368 3383 3402 PV 2 2972967 67068725 96.85% 17.304%

71 23.109 3402 3409 3426 W 2 34158 759524 1.10% 0.196% 72 24.678 3669 3676 3682 PV 2 7531 132237 0.19% 0.034% 73 25.089 3737 3746 3756 PV 2 4701 88165 0 ..13% 0.023% 74 26.394 3962 3968 3975 PV 3 5386 103895 0.15% 0.027% 75 27.951 4222 4233 4239 BV 3 4286 77154 0.11% 0.020%

76 29.396 4471 4479 4487 PV 2 4260 81339 0.12% 0.021% 77 29.978 4573 4578 4589 PV 4 2966 84427 0.12% 0.022% 78 30.066 4589 4593 4598 PV 4 2017 34749 0.05% 0.009% 79 30.812 4703 4720 4753 PV 2 2325164 56887551 82.15% 14.678% 80 31.012 4753 4754 4761 W 4 4912 109223 0.16% 0.028%

81 31.059 4761 4762 4769 W 6 3474 86592 0.13% 0.022% 82 31.376 4809 4816 4827 W 3 6171 178438 0.26% 0.046% 83 32.034 4922 4928 4937 PV 2 3845 81658 0.12% 0.021% 84 33.233 5126 5132 5139 PV 2 3341 71940 0.10% 0.019% 85 34.361 5318 5324 5339 PV 6 3388 80517 0.12% 0.021%

86 34.713 5366 5384 5422 PV 2 1652807 42580156 61.49% 10.986% 87 34.943 5422 5423 5425 W 2 5249 60817 0.09% 0.016%

10809.D 050102.M Thu May 16 12:37:11 2002 Page 2

NYC-WTC_000045990

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NYC-WTC_000045990Source: NYC Law Department, mirrored locally

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Gas chromatography-mass spectrometry report for sample AE10811 showing detection of unknown compounds and surrogate recovery.

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