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Portal Document ucAcation Report (QT Reviewed)
NYC 9/11 Public
Data File C:\MSDCHEM\l\DATA\051402\CAL20.D Vial: 15
Acq On 15 May 2002 1:44 am Operator: Mclean
Sample Inst : Instrumen
• Mise Multiplr: 1.00
MS Integration Params: EVENTS.E
Quant Time: May 16 14:20:06 2002 Quant Results File: 050102.RES
Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
ast Update : Thu May 16 12:34:41 2002
esponse via : Initial Calibration
ataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 9.93 152 6454216 40.00 ug/L 0.00
10) Napthalene-d8 13.43 136 26307538 40.00 ug/L 0.00
17) Acenapthalene-dlO 18.57 164 14704551 40.00 ug/L 0.00
29) Phenanthranene-dlO 22.96 188 22143802 40.00 ug/L 0.00
’.7) Chrysene-dl 2 30.82 240 17250856 40.00 ug/L 0.01
3) Perylene-dl2 34.71 264 13486435 40.00 ug/L 0.00
stem Monitoring Compounds
7) TCMX 20.54 209 1102170 12.35 ug/L 0.00 Cl
O
’•piked Amount 10.000 Recovery = 123.50% O
O
get Compounds Qvalue CO
<
' n-nitros-dimethyl amine 3.84 74 2551065 19.29 ug/L 87
O
bis(2-Chloroethyl)ether 9.35 93 5298931 20.98 ug/L 88 O
1,3-Dichlorobenzene 9.76 146 5140353 19.99 ug/L 99 <r
1,4-Dichlorobenzene 9.98 146 5620365 21.26 -ug/L 100
1,2-Dichlorobenzene 10.35 146 5015814 21.34 ug/1 99 O
2,2'oxybis(1-Chloropropane 10.81 45 8283524m 21.28 ug/L
N-nitroso-di-propylamine 11.14 70 3760811 21.01 ug/L 96 7
(
Hexachloroethane 11.26 117 2106818 21.61 ug/L 92 3N 2
Nitrobenzene 11.49 77 5267578 20.70 ug/L 96
isophorone 12.21 82 9897911 21.59 ug/L 99 2
is(2-Chloroethoxy) methan 12.95 93 6479458 21.33 ug/L 98 8
'6'
,2,4-Trichlorobenzene 13.30 180 4194279 21.76 ug/L 98
apthalene 13.49 128 15155537 21.50 ug/L 98
exachlorobutadiene 13.93 225 2001103 22.16 ug/L 99
-Chloronaphthalene 16.93 162 7991533 21.31 ug/L 98 %
methylphthalate 18.01 163 9915873 20.63 ug/L 99 o
O
6-Dinitrotoluene 18.12 165 1682513 22.27 ug/L 92
) 0
enapthylene 18.13 152 13978256 20.16 ug/L 98 \ w
napthalene 18.66 153 8615844 21.55 ug/L 98 \ O
l -Dinitrotoluene
thylphthalate
19.28
20.15
165 2022313
149 9058351
18.91 ug/L 95 8< Q
21.68 ug/L 98 j \ o
hlorophenyl-phenylether 20.33 204 4783874 21.66 ug/L 99 . Cl
rene 20.20 166 10035764 21.94 ug/L 98 A —4,
Q
enzene 20.78 77 11550091 20.94 ug/L 94 s o
rosodiphenylamine 20.70 169 4908215 18.06 ug/L 93
omophenyl-phenylether 21.76 248 2471890 22.60 ug/L 98
chlorobenzene 21.79 284 2313827 22.10 ug/L 99
anthrene 23.02 178 14403576 21.56 ug/L 97
'acene 23.17 178 14514180 21.24 ug/L 98
butylphthalate 25.09 149 16100679 21.95 ug/L 99
ifier out of range (m) = manual integration
50102.M Thu May 16 14:20:40 2002 Page 1
NC-WTC_000045976
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