GCMS reference results for sample AE10809, May 2002

Z K Quantitation Report (QT Reviewed) o Z © — K Data File C:\MSDCHEM\1\DATA\0514 02\CAL5 0B.D Vial: 2 O “0 Acq On 15 May 2002 10:44 am 2 -1 Sample 5/7 kb Operator: Mclean Inst : Instrumen C O o o' 1 Mise Multiplr: 1.00 “0 o o o o MS Integration Params: EVENTS.E Quant Time: May 16 14:23 2002 0 O Quant Results File: 050102.RES O CH o CD 00 N Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) 2 Title : 508 Modified GC/MS scan 3 CD Last Update : Thu May 16 12:34:41 2002 3 Response via : Initial Calibration Abundance TIC: CAL50B.D

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§88 I184* i £3 5 g ls ss ® @

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2500000 it A fl 5 8 S c t& f p § CD CD 98 A (C (o

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J; 18 5 8 o I c 2 2 2 Q a 8&08 18 ~ ! CD 2 12 2000000

IS ! 8 8 s !i 1500000 i N N o I 1000000 t “ 8

3 9 500000

0 • kl 1/*t ....... Il i ¥' i 1 1 ■ r I ■ — , i , L, a v f ,j V -----I Oku V , - Time-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00

CAL50B.D 050102.M Thu May 16 14:23:22 2002 Page 3