GCMS reference analysis results for sample AE09329, May 7 2002

Z K Z Quantitation Report (QT Reviewed) o K CD o Data File C:\MSDCHEM\1\DATA\050202\0429REFB.D Vial: 8 5-1 Acq On 2 May 2002 5:17 pm Operator: Mclean U C o Sample Inst Instrumen O 1 a o Mise Multiplr: 1.00 O “0 o o o MS Integration Params: EVENTS.E — Quant Time: May 7 11:44 2002 Quant Results File: 050102.RES 0 & O 00 o o Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) 2 Title : 508 Modified GC/MS scan § CD Last Update : Tue May 07 09:57:23 2002 3- Response via : Initial Calibration Abundance TIC: 0429REFB.D o

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2000000 | i (5 8 c 8 O 1800000 TO

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I sl g 1000000 ill it !Mi|| s 68 8 88 61 l8 2O 5 i 1 c 11 i R s ! L 8 § TO 95 2 800000 66 2 28*529 -828 83 Do Q

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400000 I i N N 2 ! in

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0 ................i—L UiULJL Lit LA 1 1 ■ । 1 r 11 ■' i 1 ■> Tr —U JW— Is Time-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00

0429REFB.D 050102.M Tue May 07 11:44:17 2002 Page 3