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GCMS analysis results for sample AE10776, May 2002

Machine-extracted title · confidence 50%

Gas chromatography-mass spectrometry report for sample AE10776 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000045890–000045898

Folder label: “GCMS X 5/6/02 A 5/11/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\MAY1002\10776.D Vial: 20 Acq On : 11 May 2002 7:37 am Operator: Sample : GC/MS SCAN 5/6 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.144 335 339 365 rBV 442712 971239 21.43% 4.311% 2 12.167 772 778 793 rBV 1405083 3213591 70.90% 14.264% 3 15.795 1168 1174 1191 rBV 1977843 4040124 89.14% 17.932% 4 21.101 1747 1753 1769 rBV 2085073 4532350 100.00% 20.117% 5 23.245 1977 1987 1995 rBV 207956 417687 9.22% 1.854%

6 25.555 2232 2239 2249 rBV2 1947532 4219158 93.09% 18.727% 7 33.619 3112 3119 3138 rBV 1299552 2915579 64.33% 12.941% 8 37.852 3572 3581 3598 rBV 734744 2219975 48.98% 9.854%

Sum of corrected areas: 22529703

10776.D GCMS0510.M Mon May 13 15:05:40 2002

NYC-WTC_000045895

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NYC-WTC_000045895Source: NYC Law Department, mirrored locally

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