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GCMS analysis results for sample AE10773, May 2002

Machine-extracted title · confidence 50%

Gas chromatography-mass spectrometry report for sample AE10773 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000045859–000045868

Folder label: “GCMS X 5/6/02 A 5/11/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\MAY1002\10773.D Vial: 17 Acq On : 11 May 2002 4:40 am Operator: Sample : GC/MS SCAN 5/6 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.136 334 338 367 rVB 436897 970881 23.37% 4.663% 2 12.159 772 777 794 rVB 1303557 2976219 71.65% 14.296% 3 14.770 1057 1062 1067 rVB 23248 43255 1.04% 0.208% 4 15.797 1168 1174 1191 rBV 1829397 3743677 90.13% 17.982% 5 21.102 1746 1753 1770 rBV 2003670 4153691 100.00% 19.951%

6 23.247 1978 1987 1994 rBV 186468 395390 9.52% 1.899% 7 25.547 2232 2238 2249 rW2 1760966 3772321 90.82% 18.120% 8 33.620 3112 3119 3134 rBV 1158568 2642892 63.63% 12.695% 9 33.840 3138 3143 3157 rVB 33669 92708 2.23% 0.445% 10 37.844 3571 3580 3599 rBV2 679284 2028033 48.82% 9.741%

Sum of corrected areas: 20819067

10773 .D GCMS0510.M Mon May 13 14:27:18 2002

NYC-WTC_000045864

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NYC-WTC_000045864Source: NYC Law Department, mirrored locally

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