NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\MAY1002\LBA.D Vial: 13
Acq On : 11 May 2002 12:46 am Operator:
Sample : GC/MS SCAN 5/6 Inst : 209
Mise : Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: May 13 12:39 2002 Quant Results File: GCMS0510.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Mon May 13 12:35:42 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0507
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.16 152 572175 40.00 ug/1 -0.04
10) Naphthalene-d8 15.80 136 2056919 40.00 ug/1 -0.04
17) Acenaphthene-dlO 21.10 164 1131008 40.00 ug/1 -0.04
30) Phenanthrene-dlO 25.55 188 1536487 40.00 ug/1 -0.03
38) Chrysene-dl 2 33.62 240 974481 40.00 ug/1 -0.02
44) Perylene-dl2 37.84 264 649798 40.00 ug/1 -0.02
System Monitoring Compounds
28) TCMX 23.25 209 37974 6.75 ug/H—-0. 03
Spiked Amount 10.000 Recovery = (67.50% —
Target Compounds Qvalue
2) N-nitrosodimethylamine 5.32 74 950 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 13.39 77 787 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.85 128 189 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 21.35 165 178 N.D.
25) Diethylphthalate 22.59 149 1610 N.D.
26) 4-Chlorophenylphenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
29) Azobenzene 0.00 77 0 N.D.
31) N-Nitrosodiphenylamine 0.00 168 0 N.D.
32) 4-Bromophenylphenylether 0.00 248 0 N.D.
33) Hexachlorobenzene 0.00 284 0 N.D.
34) Phenanthrene 25.56 178 496 N.D.
(#) = qualifier out of range (m) = manual integration
LBA.D GCMS0510.M Mon May 13 12:42:27 2002 Page 1
NYC-WTC_000045830
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