GCMS sample analysis results for AE10700, May 20 2002

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Laboratory report detailing GC/MS analysis of sample AE10700 including surrogate recovery data in May 2002.

NYC-WTC_000045735–000045747

Folder label: “GCMS X 5/3/02 A 5/13/02”

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NYC 9/11 Public Portal Document wpULL RCpUL

Data File : C:\MSDCHEM\l\DATA\020513\10700.D Vial: 11 Acq On : 13 May 2002 10:25 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 6.13 0.50 ug/1 37857 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

—1 2-Propanone, 1,1,1 - trichloro- 160 C3H3C130 000918-00-3 53 2 1-Flubrononane 146 C9H19F 000463-18-3 12 3 Decanoic acid, hexyl ester 256 C16H3202 010448-26-7 9 4 2H-Pyran-2-one, tetrahydro-4,6,6... 142 C8H14O2 020628-36-8 9 Abundance Scan 519 (6.128 min): 10700.D (-514) (-) m/ z 43.10 100.00% 43 ft 5000

''। t । ' 1 ' । । ।।' n11 । । । ।

61 84 97 110 127 5.80 6.00 6.20 6.40 ,. ,i ii nl. 1, __________ 209 267 1 1 i 1 1 ' ■ I 1 1 ‘ ' 1 1 1 1 1 I 1 । ' । ' ' ' ' । । । । ' ' 1 I ' ' ' 1 I 1 1 rrl’’ i > . । . pi-1 i i | '-r m/z 127.00 10.51% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #3877: 2-Propanone, 1,1,1-trichloro- 43

5000 ........................ A5.80 6.00 6.20 6.40 m/z 84.00 10.40% 15 27 63 83 97 110 125 - 14 ' r + ■ " 1 ' 1 p'1 1 " ■ ■ ' ■ i 1 . ' । । । । । । । । । । । । i । । । । । । । । । । । । । । । । । । । । m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #4248:1-Fluorononane 43

55 5.80 6.00 6.20 6.40 5000 29 m/z 125.00 10.21%

1 70 84 97

m/z-> 15 ‘ 1 i 1 20 l + 40 u 60 80 111 126 146 T’**1111*11*11’01111—*10’ ’IO—UT—TT 100 120 140 160 180 200 220 240 260 Abundance 43 #4129: Decanoic acid, hexyl ester 1 1 1 1 1 ,144.., i ■ ' ' 1 i 5.80 6.00 6.20 6.40 m/z 42.20 7.58% 29 5000 55 84 69 173 . ।। . 44LL 97 115 129 143155 1 ''"i"1 1 3 '! J ' i . ' | 1 1 ' | 1180185 199 213 256 ' i ' ■ 1 ‘ i ' ' 1 ' i 1 1 1 1 i ' 1 ■ ■ i 1 1 TTfTTTMf m/z-> 20 40 60 80 100 120 140 160 200 220 240 260 5.80 6.00 6.20 6.40

10700.D SCAN020507.M Wed May 15 08:39:45 2002 Page 3

NYC-WTC_000045741

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Laboratory report detailing GC/MS analysis of sample AE10698 including surrogate recovery data in May 2002.

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