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GCMS sample analysis results for AE10700, May 20 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GC/MS analysis of sample AE10700 including surrogate recovery data in May 2002.

NYC-WTC_000045735–000045747

Folder label: “GCMS X 5/3/02 A 5/13/02

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NYC 9/11 Public Portal Document UDU Hied rercent Keporc

Data File : C:\MSDCHEM\l\DATA\020513\10700.D Vial: 11 Acq On : 13 May,2002 10:25 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.7 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. . corr. % of # min scan scan scan TY height area % max. total

1 6.128 514 519 520 rBV2 25582 37857 0.89% 0.164% 2 6.158 520 524 549 rVB 474025 905595 21.41% 3.926% 3 11.375 1396 1412 1434 rBV 1222451 3038221 71.82% 13.171% 4 16.534 2275 2290 2309 rBV 1471635 3803281 89.91% 16.487% 5 24.460 3624 3639 3655 rBV2 1449702 3982818 94.15% 17.265%

6 27.539 4150 4163 4174 rBV3 210422 571197 13.50% 2.476% 7 28.362 4293 4303 4312 rVB4 12818 38370 0.91% 0.166% 8 31.094 4757 4768 4783 rVB3 10303 31792 0.75% 0.138% 9 31.717 4857 4874 4897 rBV2 1401806 4230098 100.00% 18.337% 10 31.952 4905 4914 4924 rVB3 12905 36510 0.86% 0.158%

11 32.187 4947 4954 4970 rVB2 10941 34340 0.81% 0.149% 12 39.931 6260 6272 6289 rBV2 1935350 3758990 88.86% 16.295% 13 43.156 6811 6821 6842 rBV 1317505 2599284 61.45% 11.268%

Sum of corrected areas: 23068353

10700.D SCAN020507.M Wed May 15 08:39:40 2002 Page 1

NYC-WTC_000045739

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NYC-WTC_000045739Source: NYC Law Department, mirrored locally

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