GCMS sample analysis results for AE10604, May 10 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050702\10604 .D Vial: 9 Acq On 7 May 2002 7:39 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 Cyclononasiloxane, octadeca... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 35.42 0.39 ug/L 326750 Perylene-dl2 34.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclononasiloxane, octadecamethyl- 666 C18H5409Si9 000556-71-8 90 2 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H30O2S14 004342-25-0 37 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 35 4 Pentasiloxane, dodecamethyl- 384 C12H3604Si5 000141-63-9 35 Abundance Scan 5505 (35.424 min): 10604.D (-5494) (-) m/ z 73.10 100.00% 73 A 147 221 5000 281 355 nMYMAANMAMMMM, MMP 429 35.00 35.20 35.40 35.60 35.80

/z-> 43 ■ ■ 1 1 1 ■ 1 50 1 1 1 I ' 1 ' 1 1 1 100 150 | 141 i I 1 , ........ | .... I 503 ................ TIFTT 1 1 1 1 t r r । j i 1 1 । i r t i । n m 1 t 200 250 300 350 400 450 500 550 B t । 1 । 1 । 1 । । n 600 650 m/z 147.10 74.96% Abundance #115158: Cyclononasiloxane, octadecamethyl- 73 147 221 429

355 ....................... A) MA A A................... 5000 281 35.00 35.20 35.40 35.60 35.80 m/Z 221.10 68.13% 475 I I I I I I I I I i — _ 11 I ' 1 — - vI I I T”1 | I I I 651 I I I

m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #87890: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 147 221

73 35.00 35.20 35.40 35.60 35.80 5000 m/z 281.00 36.79% 191 117 279 28 1 250 [ ' 1 ''11 ■ । ■ 1 ■ r1 ' i ' ' ' ' 1 1 ' 1 ■ i ' ■ ■ ■ i ' ■ ■ 1 1 1 ' ' ■ i ' ■ 1 ■ 1 1 ■ • ■ । ■ i r ■ Tl/Z-> Abundance 50

73 100 150 200 250 300 350 #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime... 147 400 450 500 550 600 650 «"MpM?Y MYn 35.00 35.20 35.40 35.60 35.80 m/z 355.00 28.05% 281 5000

369

m/z-> -+ 27 1

50 117 TId 100 150 207 20 . 1771, 24%, 200 250 338 | 1 | 1 ' 1 1 | 300 350 . 1 । , , , , । < , , , । 400 450 500 , 1 | I ! I 1 | | | | | | ' ! 550 600 650 ___________ ____________ | । । ' । 11 । 1 ", if 1 i । r*i । 1 ] i r 35.00 35.20 35.40 35.60 35.80

10604.D 050102.M Thu May 09 09:08:45 2002 Page 14

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