Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11904.
NYC-WTC_000012937–000012965Folder label: “GCMS X 5-21-02 A 5-22-02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11904.D Vial: 11 Aoq On : 22 May 2002 9:58 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan 15 Library- : C:\DATABASE\NIST98.L Peak Number 16 Cyclononasiloxane, octadeca... Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T. 34.33 1.06 ug/L 561495 Perylene-d12 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qu 1 Cyclononasiloxane, octadecamethyl- 666 C18H5409Si9 000556-71-8 9 2 1,1,1,5,7,7,7-Heptamethy1-3,3-bi. . . 444 C13H40O5Si6 038147-00-1 4 3 Octasiloxane, 1,1,3,3,5,5,7,7,9,... 578 C16H50O7Si8 019095-24-0 32 4 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H44O6Si7 019095-23-9 17 Abundance Scan 5318 (34.325 min): 11904.D (-5310) (-) m/ z 73.10 100.00%! 73 147 221 5000 281 355 —— 4 AnAommA 429 34.00 34.20 34.40 34.60 40 0-Ti 1 1 1 ' th ■ i i i —HH --H 191 1 325, |... 503...... .... . m/z 147.10 67.12% miz-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #115158: Cyclononasiloxane, octadecamethyl- 73 147 221 429
355 5000 281 34.00 34.20 34.40 34.60 m/z 221.10 62.94% 475
miz-> ■ ■ ■ • i ■f ■ • i ■ • Ij 0- TII—apur 1 ____ 1 1 1 I44 1 ■ i ' ■ 1 1 i ■ 1 1 ■ i ■ • ■ ■ i ■ 50 100 150 200 250 300 350 400 450 500 550 600 650 651
Abundance #26950:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)... 73
147 / 0-, — 34.00 34.20 34.40 34.60 50001 267 m/z 281.00 40.74%l 355 429 207
0- • ■ ।,'i,11( r1 miz-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance 73 #27373: Octasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13,15,1... AAA , * A A* MAAAAAWNCWK 34.00 34 20 34.40 34.60 m/z 355.10 31.76% 5000 207 281 147 341 0 244 .117177+,+2514+311 1/4385,.429 PT 503 563 m/z—> 50 100 150 200 250 300 350 400 450 500 550 600 650 34.00 34.20 34.40 34.60
11904.D 052202.M Tue May 28 12:09:26 2002 Page 19
NYC-WTC_000012960
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NYC-WTC_000012908
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012852
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
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GCMS laboratory report for sample AE11908 detecting unknown compounds and 2,4-DDD on June 4, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013574
Laboratory report documenting GCMS analysis of sample AE11931 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012823
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014578
Laboratory report showing GCMS analysis results for sample AE12534 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013154
GCMS laboratory report for sample AE09677 detecting unknown compounds and 2,4-DDD on May 23, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012881
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11902.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023904
Laboratory report showing GC/MS analysis of sample AE10981 with surrogate recovery data for 2,4-DDD.
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NYC-WTC_000012748
Department of Environmental Protection record of GCMS results generated in late May 2002.
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Administrative log recording sample identification, drip rates, and processing details for a GCMS batch.
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Gas chromatography-mass spectrometry blank analysis for sample AE11799 showing results below method reporting limits for semivolatile organic compounds, dated May 28, 2002.
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Calibration data for gas chromatography-mass spectrometry analysis of semivolatile organic compounds recorded on May 28, 2002.
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Reference standard analysis data for gas chromatography-mass spectrometry testing of semivolatile organic compounds on May 28, 2002.
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