GCMS calibration verification for VOCs, May 9 2002

2 z Quantitation Report (QT Reviewed) K K o o co 5-1 Data File C:\MSDCHEM\l\DATA\050702\CAL20.D Vial: 2 — o Acq On 7 May 2002 1:52 pm Operator: Mclean "O I o Sample 20 Inst Instrumen C O o Mise o Multiplr: 1.00 o' o MS Integration Params: EVENTS.E "0 o CH CH O. Quant Time: May 9 9:18 2002 Quant Results File: 050102.RES — 0 O Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) o Q C Title : 508 Modified GC/MS scan 3 Last Update : Wed May 08 09:53:56 2002 CD X Response via : Initial Calibration Abundance TIC: CAL20.D 2600000

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8 n © & 2 1200000 if Ji si a i 2 I < ! i 9 285 888 185 CM

1C I f § N Q 1g & X 1000000 84810 F 8* 3 8 a CD v 2 0 O 1 2 X J 1 1 9 800000 & w | 6S 600000 2 I 8 x N N X § t 2 8 IJ E 3

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200000 i I 0 —ULL L— L— । । । i i । । । । । । । । । i i | । । i i । । । kl । “i— । i । । । i । । । । i 1 । 4 । ■7 । । । । । j । i l । । । ' । r- Time-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00

CAL20.D 050102.M Thu May 09 09:19:11 2002 Page 3