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Document / 9 pages

GCMS calibration table for sample AE09449, May 2002

Machine-extracted title · confidence 100%

Technical document displaying GCMS calibration data and compound retention times for sample AE09449 processed in early May 2002.

NYC-WTC_000045507–000045515

Folder label: “GCMS X 5/3/02 A 5/8/02

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OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\MAY0202\9449.D Vial: 8 Acq On 2 May 2002 9:39 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.089 329 333 337 rBV 27008 56296 1.14% 0.226% 2 8.163 337 341 346 rBV 384588 728595 14.70% 2.922% 3 12.195 775 781 793 rBV 1598100 3501528 70.62% 14.045% 4 15.833 1171 1178 1194 rBV 2125699 4470305 90.16% 17.931% 5 21.138 1749 1757 1778 rBV 2373069 4958038 100.00% 19.887%

6 23.273 1982 1990 1996 rVB 182132 357934 7.22% 1.436% 7 25.583 2233 2242 2253 rBV2 2174477 4674351 94.28% 18.749% 8 25.720 2253 2257 2269 rVB 20149 53404 1.08% 0.214% 9 33.647 3114 3122 3137 rBV 1506208 3434320 69.27% 13.776% 10 37.880 3573 3584 3595 rBV 892198 2695798 54.37% 10.813%

Sum of corrected areas: 24930569

9449.D GCMS0501.M Fri May 03 08:41:18 2002

NYC-WTC_000045510

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NYC-WTC_000045510Source: NYC Law Department, mirrored locally

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