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GCMS calibration data for volatile organics, sample AE10198, May 2002

Machine-extracted title · confidence 95%

Laboratory report showing gas chromatography-mass spectrometry calibration results for volatile organic compounds in sample AE10198 on May 9, 2002.

NYC-WTC_000044873–000044876

Folder label: “GCMS X 4/30/02 A 5/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\050802\CAL50.D Vial: 2 Acq On 8 May 2002 11:52 am Operator: Mclean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 08 13:59:14 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed May 08 09:53:56 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

34) Anthracene 23.18 178 23650563 50.62 ug/L 98 35) Di-n-butylphthalate 25.10 149 25837613 51.51 ug/L 100 36) Fluoroanthene 26.55 202 23900666 51.04 ug/L 98 38) Pyrene 27.18 202 23063945 49.39 ug/L 98 39) Butylbenzylphthalate 29.53 149 10100217 48.54 ug/L 98 40) Benzo(a)anthracene 30.80 228 18848604 50.69 ug/L 98 41) Bis(2-ethylhexyl )phthalate 31.39 149 13869526 49.32 ug/L 97 42) Chrysene 30.89 228 19315310m 50.17 ug/L 44) Di-n-octylphthalate 33.25 149 20206829 54.81 ug/L 98 45) Benzo(b)fluoranthene 33.76 252 16800083 55.56 ug/L 97 46) Benzo(k)fluoranthene 33.84 252 19985138 52.60 ug/L 98 47) Benzo(a)pyrene 34.57 252 14521728 48.12 ug/L 98 48) Indeno(1,2,3-cd)pyrene 37.41 276 10589539 50.05 ug/L 99 49) Dibenz(a,h)anthracene 37.53 278 12157947 54.03 ug/L 99 51) Benzo(g,h,i)perylene 38.16 276 13332354 56.43 ug/L 100

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL50.D 050102.M Thu May 09 13:34:32 2002 Page 2

NYC-WTC_000044875

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NYC-WTC_000044875Source: NYC Law Department, mirrored locally

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