GCMS calibration table for TCLP analysis, April 2002

NYC 9/11 Public Portal Document DFTPP p‘ Data File C:\HPCHEM\1\DATA\APR2 502\DFTPP.D Vial: 1 Acq On 25 Apr 2002 8:35 am Operator : Sample Inst : 209 Mise Multiplr : 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP.D 2500000

2000000

1500000

1000000

500000

_ / U________________ l......... .................. o । r 11111111111Ti j 111111 1111111111111-1 ■ । > 11111 ■' ।■ 111 ■ 111 •' ' 11 ■ ■ 11 ■ ■ ■ 1 ।' ■' ■ । ' ' ' ■ । 1 ' ' ■ । ' i 1 1 ■ 1 । ' Time--> 24.80 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 28.20 28.40 28.60 Abundance Scan 2368 (26.781 min): DFTPP.D (-) 198 300000 442 250000

200000 69 255 150000 127 51 100000 110 275 50000 224 93 0 3,1 | . 148 167181 1, 11.24) . I; . 296310323 346365 383 403 423 37 1 rr 1hp—444 111 ■ ■ ,,. m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Scan 2368

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% . Limit% Abn% Abn Pass/Fail

51 198 30 60 34.9 114528 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 45.9 150499 PASS 70 69 0.00 2 0.0 0 PASS 127 198 40 60 42.7 140041 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 328219 PASS 199 198 5 9 6.8 22440 PASS 275 198 10 30 24.1 79007 PASS 365 198 1 100 2.6 8689 PASS 441 443 0.01 100 93.4 48874 PASS 442 198 40 110 81.9 268761 PASS 443 442 17 23 19.5 52341 PASS

DFTPP.D GCMS0412.M Thu Apr 25 14:44:02 2002

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