GCMS analysis results for sample AE08756, May 2002

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40 20.688 2992 2997 3000 W 2 3669 58239 0.14% 0.025%

41 21.399 3110 3118 3123 W 4 3105 72478 0.17% 0.031% 42 22.580 3311 3319 3327 W 2 18395 365848 0.87% 0.154% 43 22.798 3351 3356 3362 PV 2 1866 40396 0.10% 0.017% 44 22.962 3372 3384 3402 PV 2 1917132 40985120 97.01% 17.264% 45 23.109 3402 3409 3419 W 22666 499240 1.18% 0.210%

46 25.101 3738 3748 3755 PV 3 2313 46738 0.11% 0.020% 47 29.519 4486 4500 4511 PV 2 5030 122886 0.29% 0.052% 48 29.983 4572 4579 4583 PV 4 3297 53295 0.13% 0.022% 49 30.812 4701 4720 4751 PV 2 1510689 36454065 86.29% 15.356% 50 31.012 4751 4754 4758 W 4 4567 101575 0.24% 0.043%

51 31.041 4758 4759 4766 W 2 3591 85246 0.20% 0.036% 52 31.388 4810 4818 4823 W 6 6332 170232 0.40% 0.072% 53 31.429 4823 4825 4835 W 5 3986 114132 0.27% 0.048% 54 31.599 4850 4854 4856 W 2 2204 34563 0.08% 0.015% 55 32.063 4927 4933 4935 W 3 2192 39438 0.09% 0.017%

56 33.003 5087 5093 5095 W 3 2462 42165 0.10% 0.018% 57 33.250 5132 5135 5137 W 3 2403 33535 0.08% 0.014% 58 33.280 5137 5140 5144 W 2835 47700 0.11% 0.020% 59 33.679 5200 5208 5213 W 7 5478 143645 0.34% 0.061% 60 34.384 5322 5328 5335 W 5 2243 60586 0.14% 0.026%

61 34.560 5354 5358 5365 PV 4 1747 42013 0.10% 0.018% 62 34.713 5365 5384 5422 W 2 1146581 30036861 71.10% 12.652% 63 34.942 5422 5423 5430 W 3 5428 130140 0.31% 0.055% 64 35.007 5430 5434 5437 W 3 3507 74673 0.18% 0.031% 65 35.230 5470 5472 5475 W 2610 28318 0.07% 0.012%

66 35.424 5497 5505 5509 W 5 3309 91396 0.22% 0.038% 67 36.358 5662 5664 5668 W 3 2450 35939 0.09% 0.015% 68 37.011 5772 5775 5777 W 3 2879 37282 0.09% 0.016% 69 38.150 5965 5969 5980 PV 2 1809 70795 0.17% 0.030% 70 38.227 5980 5982 5988 W 2 2106 38322 0.09% 0.016%

71 38.415 6005 6014 6019 PV 2 1516 25930 0.06% 0.011%

Sum of corrected areas: 237399379

8756.D 050102.M Mon May 06 14:02:51 2002 Page 2

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