GCMS reference analysis results for sample AE09329, May 8 2002

NYC 9/11 Public Portal Document

- Data File C:\MSDCHEM\1\DATA\050202\9330.D Vial: 10 Acq On 2 May 2002 6:58 pm Operator: Mclean Sample 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.156 6 13 30 BV 4 5535 112657 0.21% 0.036% 2 3.397 42 54 60 PV 3 10048 167621 0.31% 0.053% 3 3.573 81 84 86 PV 4 4478 44504 0.08% 0.014% 4 3.590 86 87 92 W 3 2447 24141 0.04% 0.008% 5 3.667 92 100 110 PV 3 10840 230005 0.42% 0.073%

6 3.743 110 113 115 W 4 3297 45851 0.08% 0.015% 7 3.784 115 120 129 W 2 7788 166995 0.31% 0.053% 8 4.025 159 161 164 W 2505 26806 0.05% 0.009% 9 4.072 164 169 172 W 4 2879 54638 0.10% 0.017% 10 4.190 186 189 193 W 3 3806 64528 0.12% 0.021%

11 4.307 203 209 214 W 5 3279 69575 0.13% 0.022% 12 4.354 214 217 220 W 3 2034 31782 0.06% 0.010% 13 4.613 254 261 267 PV 6 1873 42060 0.08% 0.013% 14 5.042 329 334 340 PV 2 11064 216064 0.40% 0.069% 15 5.089 340 342 344 W 3 2083 19348 0.04% 0.006%

16 5.130 344 349 361 W 6 5269 126520 0.23% 0.040% 17 5.518 407 415 423 PV 7 3171 119853 0.22% 0.038% 18 5.988 487 495 519 W 697750 11896590 21.84% 3.796% 19 7.028 660 672 676 W 5 1878 53062 0.10% 0.017% 20 7.180 694 698 703 W 5 2197 39054 0.07% 0.012%

21 7.727 780 791 804 W 13597 337345 0.62% 0.108% 22 8.755 961 966 970 PV 3 2196 47488 0.09% 0.015% 23 9.302 1053 1059 1060 PV 3 2580 33404 0.06% 0.011% 24 9.319 1060 1062 1065 W 1982 20487 0.04% 0.007% 25 9.595 1100 1109 1118 PV 5 4453 127703 0.23% 0.041%

26 9.672 1118 1122 1128 W 5 5337 120527 0.22% 0.038% 27 9.719 1128 1130 1132 W 2 2774 27544 0.05% 0.009% 28 9.942 1158 1168 1180 W 1975807 36873113 67.68% 11.764% 29 10.065 1184 1189 1198 W 7 7197 155416 0.29% 0.050% 30 10.265 1218 1223 1233 W 5 4801 127575 0.23% 0.041%

31 10.383 1233 1243 1252 W 8 2946 110947 0.20% 0.035% 32 11.863 1490 1495 1503 W 2 2236 38872 0.07% 0.012% 33 12.040 1520 1525 1535 BV 3 2182 40924 0.08% 0.013% 34 12.416 1584 1589 1595 W 2 4756 75836 0.14% 0.024% 35 12.521 1605 1607 1613 W 3 1874 32924 0.06% 0.011%

36 12.727 1636 1642 1648 W 3 2221 47025 0.09% 0.015% 37 13.438 1750 1763 1777 W 2522401 49784760 91.38% 15.884%

9330.D 050102.M Mon May 06 13:55:01 2002 Page 1

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