Laboratory report documenting GCMS analysis of sample AE06407 conducted on May 3, 2002.
NYC-WTC_000044541–000044554Folder label: “GCMS X 4/29/02 A 5/1/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\MSDCHEM\l\DATA\050102\6407.D Vial: 17 Acq On 1 May 2002 10:45 pm Operator: Mclean Sample re-ext 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 1 2-Pentanone Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T. 3.76 0.22 ug/L 151297 1,4-Dichlorobenzene-d4 9.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Pentanone 86 C5H10O 000107-87-9 9 2 Ethane-1,2-diimine, N, N‘ -diamino- 86 C2H6N4 1000197-11-5 9 3 2-Pentanone 86 C5H10O 000107-87-9 9 4 2-Butanone, 3-methyl-_____________ 86 C5H10O 000563-80-4 9 Abundance Scan 115 (3.755 min): 6407 D (-111) (-) m/ z 43.10 100.00%
L 43 MMl// 5000
40 86 , _ 51 58 63
/z-> 5 10 274 .........T,,l....... 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 all m/z 3 40 3.60 86.00 3.80 4.00 20.93% 4.20
Abundance #7171:2-Pentanone 43 mw"OHApy 5000 । ' [“n I* "i l । I । । । । > I | I I । i | i
3 40 3.60 3.80 4.00 420 86 m/ z 84.00 17.24%
m/z-> Abundance 11 5 1518 27,3134 3,9|, 50 55 ,| 62 67 | 11»I M ITI I 11111 Trmmpnrtt ] 11 58 71 11" " i" 1' i'1111 "7' r ' " i1 " 11' " 11" " I 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #3992: Ethane-1,2-diimine, N,N‘-diamino- 11" " I " wAy"MMMpAsA 43 I I I I I I ' I I I I— I_ I I I I I I I I I I I I
3 40 3.60 3.80 4.00 4.20 5000 30 m/ z 4 0.10 16.29% WMNWWMww
27 4C 58' 86 70
m/z-> 5 10 3336,1 +52+ 6164671 73 79 83 55 i"~ i'111!1 '11 r '111 " 111 " I 1 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #110097: 2-Pentanone 43 3 40 3.60 3.80 4.00 4.20 m/ z 44.10 13.49% 5000 86 58 71 27 391. mpg 1 I ' 1 ' 1 I ' 1 1 1 | 1 1 ' 1 1 11''111 ■ ■1 ■ I ■11111111111' 11" •' 11 ■11111 TT-p-rrrp-r ■ ■ । ■ ■ ■ ■ । ■ ■ . ■ ( । । । । । । > m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.40 3.60 3.80 4.00 4.20
6407.D 050102.M Thu May 02 12:26:52 2002 Page 4
NYC-WTC_000044548
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NYC-WTC_000044510
Report listing other unknown compounds and surrogate recovery data from GCMS analysis conducted on May 3 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044496
Report listing other unknown compounds and surrogate recovery data from GCMS analysis conducted on May 3 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044526
Gas chromatography-mass spectrometry analysis report for sample AE06340, conducted May 3, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045155
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10307 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044978
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10203 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044926
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10199 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023502
Laboratory report showing GC/MS analysis results for sample AE10816 including surrogate recovery data on May 14, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022795
GCMS analytical report for environmental sample AE09151 including surrogate compound data from May 15, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023531
Laboratory report page showing GC/MS analysis for sample AE10850 including surrogate recovery data on May 14, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022938
Laboratory report documenting GCMS analysis of environmental sample AE09569 conducted on May 15, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024153
Document noting low recovery in GCMS scan of sample AE10205 and subsequent re-extraction yielding 85% recovery.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023084
Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09573 conducted on May 14, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044430
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 29 and May 1, 2002.
Filed in the same folder
NYC-WTC_000044431
Fragment of a document containing unreadable text and partial headers from a DEP laboratory procedure.
Filed in the same folder
NYC-WTC_000044433
Gas chromatography-mass spectrometry blank analysis showing results below method detection limits for organic compounds.
Filed in the same folder
NYC-WTC_000044447
Instrument qualification report for DFTPP showing pass/fail status for mass spectral limits on April 30, 2002.
Filed in the same folder
NYC-WTC_000044449
Calibration data for GCMS analysis of volatile organic compounds recorded on May 2, 2002.
Filed in the same folder