GCMS analysis results for sample AE06338, May 3 2002

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LSC Area Percent Report

Data File C:\MSDCHEM\1\DATA\050102\6338.D Vial: 14 Acq On 1 May 2002 8:18 pm Operator: Mclean Sample re-ext 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.143 4 11 16 BV 3 4852 73792 0.16% 0.029% 2 3.378 47 51 55 PV 3 6516 92001 0.20% 0.036% 3 3.426 55 59 67 W 6 3677 62016 0.14% 0.024% 4 3.572 71 84 89 W 8 3154 78367 0.17% 0.030% 5 3.649 92 97 104 W 14694 246334 0.55% 0.096%

6 3.731 104 ill 115 W 5 3505 102214 0.23% 0.040% 7 3.772 115 118 122 W 3 6492 99804 0.22% 0.039% 8 4.066 161 168 170 W 4 2072 39375 0.09% 0.015% 9 4.183 185 188 191 PV 5 2099 25336 0.06% 0.010% 10 4.213 191 193 196 W 4 2202 23851 0.05% 0.009%

11 4.289 196 206 211 W 5 3361 89328 0.20% 0.035% 12 4.371 211 220 226 W 3 2559 73170 0.16% 0.028% 13 4.965 315 321 329 PV 6 2935 54378 0.12% 0.021% 14 5.035 329 333 344 W 4 5645 145860 0.32% 0.057% 15 5.124 344 348 352 W 6 3000 44042 0.10% 0.017%

16 5.435 399 401 407 W 3 1865 23928 0.05% 0.009% 17 5.517 411 415 423 W 7 2781 79485 0.18% 0.031% 18 5.594 423 428 429 W 3 2167 31613 0.07% 0.012% 19 5.617 429 432 437 W 4 3977 79882 0.18% 0.031% 20 5.981 484 494 518 W 584170 10030606 22.27% 3.903%

21 7.726 783 791' 798 PV 3 9120 196875 0.44% 0.077% 22 7.779 798 800 807 W 4 2428 46817 0.10% 0.018% 23 8.373 897 901 906 PV 4 2073 37486 0.08% 0.015% 24 8.755 960 966 979 W 4 2386 61785 0.14% 0.024% 25 9.301 1054 1059 1069 PV 5 2744 57924 0.13% 0.023%

26 9.701 1123 1127 1136 W 5 2311 47876 0.11% 0.019% 27 9.942 1155 1168 1180 PV 1667471 30961161 68.73% 12.046% 28 10.024 1180 1182 1186 W 5 1427 24323 0.05% 0.009% 29 10.265 1215 1223 1237 W 4 17199 424886 0.94% 0.165% 30 10.388 1237 1244 1259 W 8 2970 104544 0.23% 0.041%

31 11.869 1491 1496 1500 PV 6 1972 30132 0.07% 0.012% 32 12.039 1521 1525 1529 W 2 2938 43351 0.10% 0.017% 33 12.533 1601 1609 1613 W 5 2519 60489 0.13% 0.024% 34 12.727 1636 1642 1653 W 2 2107 58533 0.13% 0.023% 35 13.191 1716 1721 1728 PV 2 1757 39847 0.09% 0.016%

36 13.437 1748 1763 1776 W 2197548 41528199 92.18% 16.157% 37 13.584 1783 1788 1793 W 3 7914 151834 0.34% 0.059%

6338.D 050102.M Thu May 02 12:23:33 2002 Page 1

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